Dodecanedioyl dichloride

Base Information

• Chemical Name: Dodecanedioyl dichloride
• CAS No.: 4834-98-4
• Molecular Formula: C12H20Cl2O2
• Molecular Weight: 267.196
• Hs Code.: 2917190090
• European Community (EC) Number: 627-587-1
• DSSTox Substance ID: DTXSID40369805
• Nikkaji Number: J120.386J
• Wikidata: Q60814666
• Mol file: 4834-98-4.mol

Synonyms:Dodecanedioyl dichloride;4834-98-4;Dodecandioyldichloride;MFCD00012243;dodecanedioyl chloride;dodecanedioic acid dichloride;SCHEMBL466419;1,12-dodecanedioyl dichloride;Dodecanedioyl dichloride, 98%;DTXSID40369805;CNXXEPWXNDFGIG-UHFFFAOYSA-N;AKOS005258281;HY-W087964;CS-0128810;D2544;FT-0635457;D90080;Q60814666

Chemical Property of Dodecanedioyl dichloride

Chemical Property:

• Vapor Pressure: <0.75 mm Hg ( 20 °C)
• Refractive Index: n20/D 1.468(lit.)
• Boiling Point: 140oC0.5 mm Hg(lit.)
• Flash Point: >230 °F
• PSA: 34.14000
• Density: 1.069 g/mL at 25oC(lit.)
• LogP: 4.41820
• XLogP3: 5.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 11
• Exact Mass: 266.0840353
• Heavy Atom Count: 16
• Complexity: 183

Purity/Quality:

98%,99%, ^*data from raw suppliers

Dodecanedioyl dichloride ^*data from reagent suppliers

Safty Information:

• Hazard Codes: C
• Statements: 34-36/37
• Safety Statements: 26-27-28-36/37/39-45

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: C(CCCCCC(=O)Cl)CCCCC(=O)Cl

Technology Process of Dodecanedioyl dichloride

There total 3 articles about Dodecanedioyl dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1,12-dodecanedioic acid (693-23-2) → 1,12-dodecanedioyl dichloride (4834-98-4)

Guidance literature:

With thionyl chloride; N,N-dimethyl-formamide; for 2h; Reflux;

Reference yield:

1,14-tetradecanedioic acid (821-38-5) → 1,12-dodecanedioyl dichloride (4834-98-4)

Guidance literature:

With caprolactam; thionyl chloride; In cyclohexane; at 75 - 80 ℃; Temperature;

Reference yield:

→ 1,12-dodecanedioyl dichloride (4834-98-4)

Guidance literature:

upstream raw materials:

1,12-dodecanedioic acid

1,14-tetradecanedioic acid

Downstream raw materials:

N₁,N₁₂-diphenyldodecanediamide

7,20-dibenzyl-2,2,3,3-tetramethyl-7,20-diaza-1,4-dioxacyclodocosane-8,19-dione

α-5,15:β-10,20-bis<2,2'-(dodecanediamido)diphenyl>porphyrin

α-5,15-<2,2'-(dodecamethylenedicarboxylamino)diphenyl>:β,β-10,20-bis-(o-aminophenyl)porphyrin

Refernces

• 1、 Retey. "Synthesis of bridged cobaloximes". . p. 2747 - 2752. Retrieved 1971.
• 2、 Ishmuratov, G. Yu.,Sayakhov, R. R.,Talipov, R. F.,Vydrina, V. A.,Yakovleva, M. P.,Zileeva, Z. R.. "Synthesis of α,ω-Diketodiesters from Betulin". . p. 706 - 711. Retrieved 2021/07/31.
• 3、 -. "LIPID PRODRUGS OF PREGNANE NEUROSTEROIDS AND USES THEREOF". Paragraph 00331; 00332. . Retrieved 2020/02/23.