Benzenamine,3,3'-[1,4-butanediylbis(oxy)]bis-

Base Information

• Chemical Name: Benzenamine,3,3'-[1,4-butanediylbis(oxy)]bis-
• CAS No.: 5226-81-3
• Molecular Formula: C16H20 N2 O2
• Molecular Weight: 272.347
• Mol file: 5226-81-3.mol

Synonyms:Aniline,3,3'-(tetramethylenedioxy)di- (6CI,7CI,8CI); 1,4-Bis(3-aminophenoxy)butane; NSC244652

Chemical Property of Benzenamine,3,3'-[1,4-butanediylbis(oxy)]bis-

Chemical Property:

• Boiling Point: 505.6°Cat760mmHg
• Flash Point: 287.3°C
• Density: 1.154g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzenamine,3,3'-[1,4-butanediylbis(oxy)]bis-

There total 1 articles about Benzenamine,3,3'-[1,4-butanediylbis(oxy)]bis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

1,4-bis(3-nitrophenoxy)butane (14467-66-4) → 3,3'-(butane-1,4-diyldioxy)bisaniline (5226-81-3)

Guidance literature:

With hydrogen; palladium; In 1,4-dioxane; ethanol; at 20 ℃; for 7h; under 3000.3 Torr;

DOI:10.1016/j.bmc.2008.06.022

Reference yield: 37.0%

3,3'-(butane-1,4-diyldioxy)bisaniline (5226-81-3) + methyl iodide (74-88-4) → C22H34N2O2(2+)*2I(1-)

Guidance literature:

With potassium carbonate; In ethanol; for 2h; Heating;

DOI:10.1016/j.bmc.2008.06.022

upstream raw materials:

1,4-bis(3-nitrophenoxy)butane

Refernces