3-O-β-D-Glucopyranosyl-D-glucitol

Base Information

• Chemical Name: 3-O-β-D-Glucopyranosyl-D-glucitol
• CAS No.: 499-16-1
• Molecular Formula: C12H24O11
• Molecular Weight: 344.316
• Mol file: 499-16-1.mol

Synonyms:3-β-D-glucopyranosyl-D-glucitol;laminaribiitol;3-O-(β-D-glucopyranosyl)-D-glucitol;(2R,3R,4R,5S)-4-((2S,3R,4S,5S,6R)-3,4,5-Trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-hexane-1,2,3,5,6-pentaol;

Chemical Property of 3-O-β-D-Glucopyranosyl-D-glucitol

Chemical Property:

• Boiling Point: 788.5±60.0 °C(Predicted)
• PKA: 12.84±0.70(Predicted)
• PSA: 200.53000
• Density: 1.69±0.1 g/cm3(Predicted)
• LogP: -5.76120

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-O-β-D-Glucopyranosyl-D-glucitol

There total 17 articles about 3-O-β-D-Glucopyranosyl-D-glucitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.9%

→ lactitol (499-16-1,535-94-4,585-86-4,585-88-6,6918-47-4,20237-67-6,20237-68-7,33904-37-9,53776-84-4,53796-37-5,64162-62-5,75828-94-3,75828-95-4,79355-25-2,93779-28-3,148346-84-3,148346-85-4)

Guidance literature:

Reference yield:

Cellobiose (13360-52-6) → β-D-glucose (492-61-5) + D-sorbitol (50-70-4) + 3-O-(β-D-glucopyranosyl)-D-glucitol (499-16-1)

Guidance literature:

With hydrogen; ruthenium; In water; at 120 ℃; for 12h; under 30002.4 Torr; pH=10.0; Further Variations:; Catalysts; pH-values; Product distribution;

DOI:10.1021/ja062468t

Reference yield:

→ lactitol (499-16-1,535-94-4,585-86-4,585-88-6,6918-47-4,20237-67-6,20237-68-7,33904-37-9,53776-84-4,53796-37-5,64162-62-5,75828-94-3,75828-95-4,79355-25-2,93779-28-3,148346-84-3,148346-85-4)

Guidance literature:

With water; nickel; at 150 ℃; under 102971 Torr; Hydrogenation;

DOI:10.1002/hlca.19370200110 DOI:10.1021/ja01270a020

upstream raw materials:

lactobionolactone

water

LACTOSE

methanol

Downstream raw materials:

lactitol nonaacetate

2-azidoethyl β-D-galactopyranosyl-(1->4)-β-D-glucopyranoside

β-D-galactopyranosyl-(1->4)-(1-deoxy-D-glucityl)-(1->N)-S²-(trityl)cysteamine

Acetic acid (2R,3S,4R,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-[(1R,2R,3S)-2,3,4-triacetoxy-1-((R)-1,2-diacetoxy-ethyl)-butoxy]-tetrahydro-pyran-3-yl ester

Refernces

• 1、 -. "Method of preparing lacitol monohydrate and dihydrate". . . Retrieved 2008/06/13.
• 2、 Sigurskjold, Bent W.,Haunstrup, Ib,Bock, Klaus. "Hydrolysis of Substrate Analogues Catalysed by β-D-Glucosidase from Aspergillus niger. Part III. Alkyl and Aryl β-D-Glucopyranosides". . p. 451 - 458. Retrieved 2007/10/02.