2,4-Dimethyl-1,3-dioxolane-2-methanol

Base Information

• Chemical Name: 2,4-Dimethyl-1,3-dioxolane-2-methanol
• CAS No.: 53951-43-2
• Molecular Formula: C6H12O3
• Molecular Weight: 132.159
• Hs Code.: 2932999099
• Mol file: 53951-43-2.mol

Synonyms:1,3-Dioxolane-2-methanol,2,4-dimethyl;1,3-Dioxolane-2-methanol, 2,4-dimethyl-;2,4-dimethyl-1,3-dioxolane-2-methanol;

Chemical Property of 2,4-Dimethyl-1,3-dioxolane-2-methanol

Chemical Property:

• Boiling Point: 180.6±15.0 °C(Predicted)
• PKA: 14.83±0.10(Predicted)
• PSA: 38.69000
• Density: 1.034±0.06 g/cm3(Predicted)
• LogP: 0.13020

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 2,4-Dimethyl-2-methylol-1,3-dioxolane is a useful research reagent for organic synthesis and other chemical processes.

Technology Process of 2,4-Dimethyl-1,3-dioxolane-2-methanol

There total 2 articles about 2,4-Dimethyl-1,3-dioxolane-2-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

propylene glycol (57-55-6,63625-56-9) → hydroxy-2-propanone (116-09-6) + (2,4-dimethyl-1,3-dioxolan-2-yl)methanol (53951-43-2)

Guidance literature:

With sodium bromate; sodium hydrogensulfite; In water; acetonitrile; at 20 ℃; for 2.5h;

DOI:10.1246/bcsj.70.2561

Reference yield:

propylene glycol (57-55-6,63625-56-9) → acetic acid (64-19-7,77671-22-8) + hydroxy-2-propanone (116-09-6) + (2,4-dimethyl-1,3-dioxolan-2-yl)methanol (53951-43-2)

Guidance literature:

With diamine-stabilized palladium nanoparticles; air; In hexane; water; at 120 ℃; for 18h; under 15001.5 Torr; Catalytic behavior; Autoclave; Sealed tube;

DOI:10.1002/cctc.202100309

upstream raw materials:

propylene glycol

Refernces

• 1、 Sakaguchi, Satoshi,Kikuchi, Daisuke,Ishii, Yasutaka. "Oxidation of Diols and Ethers by NaBrO3/NaHSO3 Reagent". . p. 2561 - 2566. Retrieved 2007/10/03.