((9-Oxo-9H-thioxanthen-2-yl)oxy)acetic acid

Base Information

• Chemical Name: ((9-Oxo-9H-thioxanthen-2-yl)oxy)acetic acid
• CAS No.: 84434-05-9
• Molecular Formula: C15H10O4S
• Molecular Weight: 286.308
• Hs Code.: 2932999099
• European Community (EC) Number: 282-803-8
• UNII: BU3L3YF2NY
• DSSTox Substance ID: DTXSID60233397
• Nikkaji Number: J297.668D
• Wikidata: Q83114902
• Mol file: 84434-05-9.mol

Synonyms:84434-05-9;((9-Oxo-9H-thioxanthen-2-yl)oxy)acetic acid;[(9-oxo-9H-thioxanthen-2-yl)oxy]acetic acid;2-(9-oxothioxanthen-2-yl)oxyacetic acid;BU3L3YF2NY;EINECS 282-803-8;2-(Carboxymethoxy)thioxanthone;UNII-BU3L3YF2NY;2-carboxymethoxythioxanthone;2-((9-Oxo-9H-thioxanthen-2-yl)oxy)acetic acid;(9-oxo-9H-thioxanthen-2-yloxy)acetic acid;Acetic acid, 2-[(9-oxo-9H-thioxanthen-2-yl)oxy]-;ACETIC ACID, 2-((9-OXO-9H-THIOXANTHEN-2-YL)OXY)-;2-thioxanthonyloxyacetic acid;SCHEMBL112717;DTXSID60233397;LJUKODJASZSKFL-UHFFFAOYSA-N;2-Carboxymethoxythioxanthone (Cmtx);AMY39898;2-(Carboxymethoxy)-9H-thioxanthene-9-one;F88138

Chemical Property of ((9-Oxo-9H-thioxanthen-2-yl)oxy)acetic acid

Chemical Property:

• Appearance/Colour: yellow powder
• Vapor Pressure: 5.13E-12mmHg at 25°C
• Refractive Index: 1.685
• Boiling Point: 528.9 °C at 760 mmHg
• Flash Point: 273.7 °C
• PSA: 91.84000
• Density: 1.415 g/cm³
• LogP: 2.87810
• Water Solubility.: 18.6mg/L at 20℃
• XLogP3: 3.6
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 3
• Exact Mass: 286.02997997
• Heavy Atom Count: 20
• Complexity: 397

Purity/Quality:

99.9% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)C(=O)C3=C(S2)C=CC(=C3)OCC(=O)O

Technology Process of ((9-Oxo-9H-thioxanthen-2-yl)oxy)acetic acid

There total 7 articles about ((9-Oxo-9H-thioxanthen-2-yl)oxy)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.91%

2-hydroxy thioxanthone (31696-67-0) + ethyl bromoacetate (105-36-2) → 2-[(9-oxo-9H-thioxanthen-2-yl)oxy]-acetic acid (84434-05-9)

Guidance literature:

2-hydroxy thioxanthone; With sodium hydroxide; In tetrahydrofuran; for 1.5h; Reflux;

ethyl bromoacetate; In tetrahydrofuran; at 40 ℃; for 4h; Reflux;

Reference yield: 80.0%

Thiosalicylic acid (147-93-3) + 2-phenoxyacetic acid (122-59-8) → 2-[(9-oxo-9H-thioxanthen-2-yl)oxy]-acetic acid (84434-05-9)

Guidance literature:

Thiosalicylic acid; With sulfuric acid; for 0.0833333h;

2-phenoxyacetic acid; at 80 ℃; for 2h;

DOI:10.1016/j.jphotochem.2018.03.024

Reference yield: 76.0%

2,2'-dithiobenzoic acid (119-80-2) + 2-phenoxyacetic acid (122-59-8) → 2-[(9-oxo-9H-thioxanthen-2-yl)oxy]-acetic acid (84434-05-9)

Guidance literature:

With sulfuric acid; at 0 - 25 ℃; for 1h;

upstream raw materials:

Thiosalicylic acid

2-phenoxyacetic acid

2,2'-dithiobenzoic acid

2-hydroxy thioxanthone

Refernces

• 1、 Batibay, Gonul S.,Gunkara, Omer Tahir,Ocal, Nuket,Arsu, Nergis. "In-situ photoinduced formation of self–assembled Ag NPs using POSS-TX as nano-photoinitiator in PEGMEA/PEGDA polymer matrix and creating self-wrinkled pattern". . p. 73 - 79. Retrieved 2018.
• 2、 -. "WATER-BASED UV INKJET INK". Paragraph 0071. . Retrieved 2015/12/17.