1,3-Benzenediol, 2,4,6-trinitro-, lead(2+) salt (1:1), monohydrate

Base Information

• Chemical Name: 1,3-Benzenediol, 2,4,6-trinitro-, lead(2+) salt (1:1), monohydrate
• CAS No.: 66778-13-0
• Molecular Formula: C6H3N3O8.H2O.Pb
• Molecular Weight: 468.305
• Mol file: 66778-13-0.mol

Synonyms:

Chemical Property of 1,3-Benzenediol, 2,4,6-trinitro-, lead(2+) salt (1:1), monohydrate

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,3-Benzenediol, 2,4,6-trinitro-, lead(2+) salt (1:1), monohydrate

There total 10 articles about 1,3-Benzenediol, 2,4,6-trinitro-, lead(2+) salt (1:1), monohydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ lead styphnate monohydrate (66778-13-0)

Guidance literature:

With lead(II) nitrate; acetic acid; bei Siedetemperatur;

Reference yield:

lead(II) nitrate + styphnic acid (82-71-3) → lead styphnate monohydrate (66778-13-0)

Guidance literature:

With ethanolamine; In ethanol; water; to soln. of styphnic acid in ethanol added soln. of Pb(NO3)2 in H2O; mixt. heated to 70°C; ethanolamine added dropwise with stirring to pH 3.5; ethanol added and mixt. brought back to temp.; soln. ethanolamine in ethanol added dropwise to pH 4.8; ppt. filtered off; washed (H2O); dried; elem. anal.;

DOI:10.1016/0040-6031(94)85003-8

Reference yield:

12-amino-abieta-8,11,13-trien-18-oic acid methyl ester; hydrochloride → lead styphnate monohydrate (66778-13-0)

Guidance literature:

at 80 ℃; under 9 Torr;

DOI:10.1021/ja01878a080

upstream raw materials:

ethanol

styphnic acid

lead acetate

ent-17-acetoxy-1-acetyl-4ξ-methyl-15β(or 20α)H-coryn-18-enium; chloride

Downstream raw materials:

cis-abienol