Technology Process of Piperidine, 2-butyl-
There total 1 articles about Piperidine, 2-butyl- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
diethyl ether;
for 1.16667h;
Ambient temperature;
DOI:10.1021/jo01296a036
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 88 percent / K2CO3 / acetonitrile / 20 h / Heating
2: 90 percent / 1,4-dicyanonaphthalene, methyl viologen / acetonitrile / 4 h / Irradiation
3: 96 percent / diethyl ether / 0.5 h / Ambient temperature
4: 1.) α-chloroethyl chloroformate, 2.) MeOH / 1.) CH2Cl2, reflux, 2.) reflux, 1 h
5: acetonitrile / 12 h / Heating
With
methanol; carbonochloridic acid 1-chloro-ethyl ester; naphthalene-1,4-dicarbonitrile; Paraquat; potassium carbonate;
In
diethyl ether; acetonitrile;
DOI:10.1016/S0040-4020(01)80497-X