4-Octene, 4-chloro-, (Z)-

Base Information

• Chemical Name: 4-Octene, 4-chloro-, (Z)-
• CAS No.: 7321-48-4
• Molecular Formula: C8H15Cl
• Molecular Weight: 146.66
• Mol file: 7321-48-4.mol

Synonyms:Z-4-chloro-4-octene;4-chloro-oct-4-ene;4-Chlor-oct-4t-en;4-Octene, 4-chloro-, (Z)-;4-chloro-oct-4t-ene;(Z)-4-chloro-oct-4-ene;4-Octene,4-chloro-,(Z);

Chemical Property of 4-Octene, 4-chloro-, (Z)-

Chemical Property:

• Refractive Index: 1.4447
• Boiling Point: 190°C (estimate)
• PSA: 0.00000
• Density: 0.9162 (estimate)
• LogP: 3.70930

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-Octene, 4-chloro-, (Z)-

There total 4 articles about 4-Octene, 4-chloro-, (Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Octyne (1942-45-6) → octan-4-one (589-63-9) + (Z)-4-Chloro-4-octene (7321-48-4)

Guidance literature:

With hydrogenchloride; at 80 ℃; for 18h; Yield given. Title compound not separated from byproducts;

DOI:10.1016/S0040-4020(01)88586-0

Reference yield:

1,2,3-trichloro-2-butene (2431-54-1) + ethylmagnesium bromide (925-90-6) → (Z)-4-Chloro-4-octene (7321-48-4) + ethane (74-84-0) + ethene (74-85-1) + (Z)-1,2-Dichloro-hex-2-ene (125101-32-8)

Guidance literature:

In diethyl ether; at 40 - 45 ℃; for 5h; Further byproducts given;

Reference yield:

1,2,3-trichloro-2-butene (2431-54-1) + ethylmagnesium bromide (925-90-6) → (Z)-4-Chloro-4-octene (7321-48-4) + ethane (74-84-0) + (Z)-1,3-Dichloro-hex-2-ene (125101-31-7) + (Z)-1,2-Dichloro-hex-2-ene (125101-32-8)

Guidance literature:

In diethyl ether; at 40 - 45 ℃; for 5h; Yield given. Further byproducts given. Title compound not separated from byproducts;

upstream raw materials:

4-Octyne

1,2,3-trichloro-2-butene

ethylmagnesium bromide

Downstream raw materials:

5-decyne

4-Octyne

Refernces

• 1、 Hudrlik, Paul F.,Kulkarni, Ashok K.,Jain, Sadhana,Hudrlik, Anne M.. "STEREOCHEMISTRY OF THE WURTZ-FITTIG PERPARATION OF VINYLSILANES". . p. 877 - 882. Retrieved 2007/10/02.