Technology Process of Boranamine, 1-chloro-N,N,1-trimethyl-
There total 1 articles about Boranamine, 1-chloro-N,N,1-trimethyl- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
neat (no solvent);
heating between 170 to 180°C;;
- Guidance literature:
-
In
diethyl ether; pentane;
byproducts: LiCl; Li-compd. in ether stirred for 1 h at -40°C with CH3BClN(CH3)2 in pentane; soln. with ppt. warmed to room temp., soln. cooled again to -40°C, evapd. in vac., solid filtered, filtrate distd.; elem. anal.;