Acetyl(m-chlorobenzoyl) peroxide

Base Information

• Chemical Name: Acetyl(m-chlorobenzoyl) peroxide
• CAS No.: 777-05-9
• Molecular Formula: C9H7ClO4
• Molecular Weight: 214.60200
• Mol file: 777-05-9.mol

Synonyms:Acetyl-m-chlorperoxybenzoat;m-Chlor-benzoyl-acetyl-peroxid;Peroxide,acetyl m-chlorobenzoyl;Peroxide,acetyl 3-chlorobenzoyl;Acetyl-<3-chlor-benzoyl>-peroxyd;

Chemical Property of Acetyl(m-chlorobenzoyl) peroxide

Chemical Property:

• PSA: 52.60000
• LogP: 1.97490

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Acetyl(m-chlorobenzoyl) peroxide

There total 3 articles about Acetyl(m-chlorobenzoyl) peroxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

acetic acid (64-19-7,77671-22-8) + 3-chlorobenzoate (535-80-8) → acetyl-(3-chloro-benzoyl)-peroxide (777-05-9)

Guidance literature:

With dmap; dihydrogen peroxide; dicyclohexyl-carbodiimide; In dichloromethane; at -10 ℃; for 3h;

DOI:10.1021/jacs.1c05881

Reference yield:

acetic anhydride (108-24-7) + m-Chlorobenzaldehyde (587-04-2) → acetyl-(3-chloro-benzoyl)-peroxide (777-05-9)

Guidance literature:

With air; Irradiation;

Reference yield:

→ acetyl-(3-chloro-benzoyl)-peroxide (777-05-9)

Guidance literature:

3-Chlor-benzaldehyd, Acetanhydrid u. O2 (Na-Acetat);

upstream raw materials:

acetic anhydride

m-Chlorobenzaldehyde

acetic acid

3-chlorobenzoate

Refernces