Technology Process of Benzenesulfonic acid, 2,4,6-tris(1-methylethyl)-,
cyclododecylidenehydrazide
There total 1 articles about Benzenesulfonic acid, 2,4,6-tris(1-methylethyl)-,
cyclododecylidenehydrazide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) s-BuLi / 1.) TMEDA, -45 deg C, 1 h; 0 deg C, 3O min 2.) TMEDA, -45 deg C, 1 h; room temp., overnight
2: 77 percent / 30percent H2O2 / tetrahydrofuran / 1.) 0 deg C, 2.) room temp., 2 h Further oxidizing agent: 40 percent peracetic acid
With
dihydrogen peroxide; sec.-butyllithium;
In
tetrahydrofuran;
DOI:10.1016/S0040-4039(01)82996-8
- Guidance literature:
-
dimethylsulfone;
With
isopropylmagnesium chloride;
In
tetrahydrofuran;
at 20 ℃;
for 1h;
cyclododecanone (2,4,6-triisopropylbenzenesulfonyl)hydrazone;
In
tetrahydrofuran;
at 20 ℃;
for 16h;
Further stages.;
DOI:10.1021/jo015699l
