1-(Allyloxy)-3-methoxypropan-2-ol

Base Information

• Chemical Name: 1-(Allyloxy)-3-methoxypropan-2-ol
• CAS No.: 28025-23-2
• Molecular Formula: C7H14 O3
• Molecular Weight: 146.186
• European Community (EC) Number: 248-786-6
• DSSTox Substance ID: DTXSID80950716
• Nikkaji Number: J250.630K
• Mol file: 28025-23-2.mol

Synonyms:1-(Allyloxy)-3-methoxypropan-2-ol;28025-23-2;EINECS 248-786-6;1-(allyloxy)-3-methoxy-2-propanol;SCHEMBL9147275;1-allyloxy-3-methoxypropan-2-ol;DTXSID80950716;LS-122490;1-Methoxy-3-[(prop-2-en-1-yl)oxy]propan-2-ol

Chemical Property of 1-(Allyloxy)-3-methoxypropan-2-ol

Chemical Property:

• Vapor Pressure: 0.0576mmHg at 25°C
• Boiling Point: 205.9°Cat760mmHg
• Flash Point: 78.4°C
• PSA: 38.69000
• Density: 0.975g/cm³
• LogP: 0.19630
• XLogP3: 0
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 6
• Exact Mass: 146.094294304
• Heavy Atom Count: 10
• Complexity: 82.9

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COCC(COCC=C)O

Technology Process of 1-(Allyloxy)-3-methoxypropan-2-ol

There total 4 articles about 1-(Allyloxy)-3-methoxypropan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

Allyl glycidyl ether (106-92-3,25639-25-2,90907-93-0) + methanol (67-56-1) → 1-(allyloxy)-3-methoxypropan-2-ol (28025-23-2)

Guidance literature:

With tin(IV)tetraphenylporphyrinato trifluoromethanesulfonate; for 0.333333h; Heating;

DOI:10.1016/j.tet.2004.05.069

Reference yield: 98.0%

1,2-epoxy-3-vinylpropane (6790-38-1) + methanol (67-56-1) → 1-(allyloxy)-3-methoxypropan-2-ol (28025-23-2)

Guidance literature:

With iodine; polyvinylpyrrolidone; at 25 ℃; for 5h;

DOI:10.1139/v97-626

Reference yield: 69.0%

Allyl glycidyl ether (106-92-3,25639-25-2,90907-93-0) + methanol (67-56-1) → 3-allyloxy-2-methoxy-1-propanol (171817-12-2) + 1-(allyloxy)-3-methoxypropan-2-ol (28025-23-2)

Guidance literature:

With aniline-terephthalaldehyde resin p-toluenesulfonate; at 20 ℃; for 24h; Reagent/catalyst;

DOI:10.1080/00397911.2016.1223309

upstream raw materials:

Allyl glycidyl ether

methanol

1,2-epoxy-3-vinylpropane

Refernces

• 1、 Smirnov et al.. "". . . Retrieved 1970.
• 2、 Olia, Fahimeh Karami,Sayyahi, Soheil,Taheri, Narges. "An Fe3O4 nanoparticle-supported Mn (II)-azo Schiff complex acts as a heterogeneous catalyst in alcoholysis of epoxides". . p. 370 - 376. Retrieved 2017/03/15.