Pyrimidinium, 4-methyl-, 1-[2-(4-iodophenyl)-2-oxoethylide]

Base Information

• Chemical Name: Pyrimidinium, 4-methyl-, 1-[2-(4-iodophenyl)-2-oxoethylide]
• CAS No.: 872691-39-9
• Molecular Formula: C13H11IN2O
• Molecular Weight: 338.148
• Mol file: 872691-39-9.mol

Synonyms:

Chemical Property of Pyrimidinium, 4-methyl-, 1-[2-(4-iodophenyl)-2-oxoethylide]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Pyrimidinium, 4-methyl-, 1-[2-(4-iodophenyl)-2-oxoethylide]

There total 3 articles about Pyrimidinium, 4-methyl-, 1-[2-(4-iodophenyl)-2-oxoethylide] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

1-[2-(4-iodophenyl)-2-oxoethyl]-4-methylpyrimidinium bromide → 4-methylpyrimidinium 2-(4-iodophenyl)-2-oxoethylide (872691-39-9)

Guidance literature:

With potassium carbonate; In ethanol; water;

DOI:10.1002/hlca.200590214

Reference yield:

4-Methylpyrimidine (3438-46-8) → 4-methylpyrimidinium 2-(4-iodophenyl)-2-oxoethylide (872691-39-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / diethyl ether / 1 h / 50 °C

2: 97 percent / K₂CO₃ / ethanol; H₂O

With potassium carbonate; In diethyl ether; ethanol; water;

DOI:10.1002/hlca.200590214

Reference yield:

2-bromo-1-(4-iodophenyl)ethanone (31827-94-8) → 4-methylpyrimidinium 2-(4-iodophenyl)-2-oxoethylide (872691-39-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / diethyl ether / 1 h / 50 °C

2: 97 percent / K₂CO₃ / ethanol; H₂O

With potassium carbonate; In diethyl ether; ethanol; water;

DOI:10.1002/hlca.200590214

upstream raw materials:

4-Methylpyrimidine

2-bromo-1-(4-iodophenyl)ethanone

Refernces