nitric acid, (7-oxo-1,8-naphthyridin-8-id-2-yl)azanide, 2-piperidin-1-id-2-ylpiperidin-1-ide, 2-piperidin-1-id-2-yl-6H-pyridin-1-ide, platinum

Base Information

• Chemical Name: nitric acid, (7-oxo-1,8-naphthyridin-8-id-2-yl)azanide, 2-piperidin-1-id-2-ylpiperidin-1-ide, 2-piperidin-1-id-2-yl-6H-pyridin-1-ide, platinum
• CAS No.: 7235-15-6
• Molecular Formula: C₁₃H₉NO₃
• Molecular Weight: 227.219
• Mol file: 7235-15-6.mol

Synonyms:Fluoren-3-ol,2-nitro- (6CI,8CI)

Chemical Property of nitric acid, (7-oxo-1,8-naphthyridin-8-id-2-yl)azanide, 2-piperidin-1-id-2-ylpiperidin-1-ide, 2-piperidin-1-id-2-yl-6H-pyridin-1-ide, platinum

Chemical Property:

• Vapor Pressure: 0.0169mmHg at 25°C
• Boiling Point: 254.8°Cat760mmHg
• Flash Point: 126.5°C
• Density: g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of nitric acid, (7-oxo-1,8-naphthyridin-8-id-2-yl)azanide, 2-piperidin-1-id-2-ylpiperidin-1-ide, 2-piperidin-1-id-2-yl-6H-pyridin-1-ide, platinum

There total 6 articles about nitric acid, (7-oxo-1,8-naphthyridin-8-id-2-yl)azanide, 2-piperidin-1-id-2-ylpiperidin-1-ide, 2-piperidin-1-id-2-yl-6H-pyridin-1-ide, platinum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2,9,9a-tetrahydro-fluoren-3-one (4590-03-8) → 2-nitro-fluoren-3-ol (7235-15-6)

Guidance literature:

Multi-step reaction with 4 steps

1: fluorene / Pd-C / Heating

2: OH^-

3: aq. HNO₃ / acetic acid

4: aq. HBr / acetic acid

With 9H-fluorene; hydrogen bromide; hydroxide; nitric acid; palladium on activated charcoal; In acetic acid;

DOI:10.1021/jm00323a018

Reference yield:

3-Hydroxy-1.4-dihydro-fluoren-2-carbonsaeure-aethylester (7263-78-7) → 2-nitro-fluoren-3-ol (7235-15-6)

Guidance literature:

Multi-step reaction with 5 steps

1: aq. HCl / ethanol / Heating

2: fluorene / Pd-C / Heating

3: OH^-

4: aq. HNO₃ / acetic acid

5: aq. HBr / acetic acid

With hydrogenchloride; 9H-fluorene; hydrogen bromide; hydroxide; nitric acid; palladium on activated charcoal; In ethanol; acetic acid;

DOI:10.1021/jm00323a018

Reference yield:

methyl-(2-nitro-fluoren-3-yl)-ether (7275-88-9) → 2-nitro-fluoren-3-ol (7235-15-6)

Guidance literature:

With hydrogen bromide; In acetic acid;

DOI:10.1021/jm00323a018

upstream raw materials:

3-hydroxyfluorene

methyl-(2-nitro-fluoren-3-yl)-ether

3-methoxyl-9H-fluorene

1,2,9,9a-tetrahydro-fluoren-3-one

Downstream raw materials:

3-hydroxy-2-aminofluorene