Hydroxylamine, N-methoxy-O-(2-methylpropyl)-

Base Information

• Chemical Name: Hydroxylamine, N-methoxy-O-(2-methylpropyl)-
• CAS No.: 88470-28-4
• Molecular Formula: C5H13NO2
• Molecular Weight: 119.164
• Mol file: 88470-28-4.mol

Synonyms:

Chemical Property of Hydroxylamine, N-methoxy-O-(2-methylpropyl)-

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Hydroxylamine, N-methoxy-O-(2-methylpropyl)-

There total 1 articles about Hydroxylamine, N-methoxy-O-(2-methylpropyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.2%

C8H18N2O3 (88470-25-1) → N-methoxy-N-isobuthoxyamine (88470-28-4)

Guidance literature:

With potassium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In water; at 20 ℃; for 4h;

DOI:10.1007/BF00955378

Reference yield: 70.1%

4-methoxymethyl-morpholine (7309-48-0) + N-methoxy-N-isobuthoxyamine (88470-28-4) → N-morpholinomethyl-N-methoxy-N-isobutoxyamine

Guidance literature:

at 20 ℃; for 48h;

DOI:10.1007/BF00955378

Reference yield: 63.5%

sodium methylate (124-41-4) + N-methoxy-N-isobuthoxyamine (88470-28-4) → N,N-dimethoxy-N-isobuthoxyamine (88470-36-4)

Guidance literature:

With tert-butylhypochlorite; In 1,2-dimethoxyethane; at -78 - -8 ℃; for 4h;

DOI:10.1016/S0040-4020(01)81731-2

upstream raw materials:

C₈H₁₈N₂O₃

Downstream raw materials:

N,N-dimethoxy-N-isobuthoxyamine

C₁₀H₂₄N₂O₄

C₅H₁₂NO₂

Refernces

• 1、 Rudchenko, V. F.,Ignatov, S. M.,Chervin, I. I.,Nosova, V. S.,Kostyanovskii, R. G.. "ASYMMETRIC NITROGEN. COMMUNICATION 48. GEMINAL SYSTEMS. COMMUNICATION 32. NH-DIALKOXYAMINES: SYNTHESIS, HYDROXY- AND AMINOMETHYLATION, NMR SPECTRA, AND CONFIGURATIONAL STABILITY". . p. 1045 - 1052. Retrieved 2007/10/02.