Technology Process of 5-(Benzyloxy)-6-methoxy-1h-indene
There total 10 articles about 5-(Benzyloxy)-6-methoxy-1h-indene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Grubbs catalyst first generation;
In
dichloromethane;
at 20 ℃;
for 2h;
DOI:10.1002/jccs.200400060
- Guidance literature:
-
With
Grubbs catalyst first generation;
In
dichloromethane;
at 20 ℃;
for 2h;
Inert atmosphere;
DOI:10.1002/jccs.200400060
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 92 percent / K2CO3 / acetone
2.1: K2CO3 / acetone
3.1: potassium tert-butoxide / tetrahydrofuran / 0.17 h
3.2: 78 percent / tetrahydrofuran
4.1: 93 percent / Grubbs catalyst / CH2Cl2 / 2 h / 20 °C
With
potassium tert-butylate; potassium carbonate;
Grubbs catalyst first generation;
In
tetrahydrofuran; dichloromethane; acetone;
2.1: Claisen rearrangement / 4.2: Wittig reaction;
DOI:10.1002/jccs.200400060