Silanamine, 1,1,1-trichloro-N,N-dimethyl-

Base Information

• Chemical Name: Silanamine, 1,1,1-trichloro-N,N-dimethyl-
• CAS No.: 13307-04-5
• Molecular Formula: C2H6 Cl3 N Si
• Molecular Weight: 178.521
• Hs Code.: 2931900090
• DSSTox Substance ID: DTXSID90157936
• Wikidata: Q83026094
• Mol file: 13307-04-5.mol

Synonyms:Silanamine, 1,1,1-trichloro-N,N-dimethyl-;13307-04-5;N-methyl-N-trichlorosilylmethanamine;trichlorosilyldimethylamine;SCHEMBL691686;N-(Trichlorosilyl)dimethylamine;DTXSID90157936

Chemical Property of Silanamine, 1,1,1-trichloro-N,N-dimethyl-

Chemical Property:

• Vapor Pressure: 18.2mmHg at 25°C
• Boiling Point: 116.4°C at 760 mmHg
• Flash Point: 24.2°C
• PSA: 3.24000
• Density: 1.287g/cm³
• LogP: 1.70000
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 176.933509
• Heavy Atom Count: 7
• Complexity: 58.4

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)[Si](Cl)(Cl)Cl

Technology Process of Silanamine, 1,1,1-trichloro-N,N-dimethyl-

There total 2 articles about Silanamine, 1,1,1-trichloro-N,N-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bis(dimethylamino)dimethylsilane (3768-58-9) → 1,1,1-trichloro-N,N-dimethylsilanamine (13307-04-5) + bis(N,N-dimethylamino)dichlorosilane (13328-30-8) + (N,N-dimethylamino)dimethylchlorosilane (18209-60-4) + dimethylsilicon dichloride (75-78-5,30107-43-8)

Guidance literature:

With tetrachlorosilane; In benzene; Product distribution; halide-NMe₂ exchange reactions were investigated; neat; other reaction partner;

DOI:10.1039/DT9810001264

Reference yield:

bis(dimethylamino)dimethylsilane (3768-58-9) → 1,1,1-trichloro-N,N-dimethylsilanamine (13307-04-5) + dimethylsilicon dichloride (75-78-5,30107-43-8)

Guidance literature:

With tetrachlorosilane; In benzene; halide-NMe₂ exchange reaction;

DOI:10.1039/DT9810001264

Reference yield:

1,1,1-trichloro-N,N-dimethylsilanamine (13307-04-5) + bis(N,N-dimethylamino)dichlorosilane (13328-30-8) → tris(dimethylamino)chlorosilane (13307-05-6)

Guidance literature:

In benzene-d6; at 23.84 ℃; Kinetics; Equilibrium constant;

DOI:10.1039/b210282j

upstream raw materials:

bis(dimethylamino)dimethylsilane

Downstream raw materials:

bis(N,N-dimethylamino)dichlorosilane

dimethylsilicon dichloride

tris(dimethylamino)chlorosilane

Refernces