Hexahydrodibenzsuberane

Base Information

• Chemical Name: Hexahydrodibenzsuberane
• CAS No.: 7351-53-3
• Molecular Formula: C15H20
• Molecular Weight: 200.324
• Mol file: 7351-53-3.mol

Synonyms:1,2,3,4,4a,10,11,11a-Octahydro-5H-dibenzocyclohepten;Hexahydrodibenzsuberane;1H-Dibenzo(a,d)cycloheptene,2,3,4,4a,5,10,11,11a-octahydro;

Chemical Property of Hexahydrodibenzsuberane

Chemical Property:

• Vapor Pressure: 0.00118mmHg at 25°C
• Boiling Point: 309.2°Cat760mmHg
• Flash Point: 135.6°C
• PSA: 0.00000
• Density: 0.972g/cm³
• LogP: 3.98170

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Hexahydrodibenzsuberane

There total 5 articles about Hexahydrodibenzsuberane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

hexahydrohomophthalic anhydride (4702-28-7,27866-85-9,71963-81-0,75829-70-8) → 1,2,3,4,4a,10,11,11a-Octahydro-5H-dibenzocyclohepten (7351-53-3)

Guidance literature:

Multi-step reaction with 4 steps

1: AlCl₃

2: N₂H₄*H₂O, NaOH / bis-(2-hydroxy-ethyl) ether

3: (i) SOCl₂, (ii) AlCl₃

4: Zn-Hg, aq. HCl / toluene

With hydrogenchloride; sodium hydroxide; aluminium trichloride; hydrazine hydrate; mercury; zinc; In toluene; diethylene glycol;

Reference yield:

5-Oxo-1,2,3,4,4a,10,11,11a-octahydro-5H-dibenzocyclohepten (7351-59-9) → 1,2,3,4,4a,10,11,11a-Octahydro-5H-dibenzocyclohepten (7351-53-3)

Guidance literature:

With hydrogenchloride; mercury; zinc; In toluene;

Reference yield:

1-Phenethyl-2-carboxy-cyclohexan (7351-57-7) → 1,2,3,4,4a,10,11,11a-Octahydro-5H-dibenzocyclohepten (7351-53-3)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) SOCl₂, (ii) AlCl₃

2: Zn-Hg, aq. HCl / toluene

With hydrogenchloride; mercury; zinc; In toluene;

upstream raw materials:

5-Oxo-1,2,3,4,4a,10,11,11a-octahydro-5H-dibenzocyclohepten

1-Phenethyl-2-carboxy-cyclohexan

1-Phenacyl-2-carboxy-cyclohexan

hexahydrohomophthalic anhydride