N,N,N',N'-TETRAETHYL-1,3-PROPANEDIAMINE

Base Information

• Chemical Name: N,N,N',N'-TETRAETHYL-1,3-PROPANEDIAMINE
• CAS No.: 60558-96-5
• Molecular Formula: C₁₁H₂₆N₂
• Molecular Weight: 186.341
• Hs Code.: 2921290000
• Mol file: 60558-96-5.mol

Synonyms:N,N,N',N'-Tetraethyl-1,3-propanediamine;

Chemical Property of N,N,N',N'-TETRAETHYL-1,3-PROPANEDIAMINE

Chemical Property:

• Appearance/Colour: clear yellow liquid
• Melting Point: 157.5-159.5 °C
• Refractive Index: n20/D 1.4377(lit.)
• Boiling Point: 206.7 °C at 760 mmHg
• PKA: 10.70±0.25(Predicted)
• Flash Point: 76.1 °C
• PSA: 6.48000
• Density: 0.829 g/cm³
• LogP: 2.06010

Purity/Quality:

99% ^*data from raw suppliers

N,N,N′,N′-Tetraethyl-1,3-propanediamine 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): C
• Hazard Codes: C
• Statements: 34
• Safety Statements: 26-27-36/37/39-45

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N,N,N',N'-TETRAETHYL-1,3-PROPANEDIAMINE

There total 2 articles about N,N,N',N'-TETRAETHYL-1,3-PROPANEDIAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetra-N-ethyl-ξ-propenediyldiamine (100536-45-6) → N,N',N,N'-tetraethyl-1,3-propanediamine (60558-96-5)

Guidance literature:

With nickel; Hydrogenation;

DOI:10.1021/ja01128a044

Reference yield:

diethylamine (109-89-7) + 1,3-dibromo-propane (109-64-8) → N,N',N,N'-tetraethyl-1,3-propanediamine (60558-96-5)

Guidance literature:

With nitromethane;

DOI:10.1080/00221340208978480

Reference yield:

N,N',N,N'-tetraethyl-1,3-propanediamine (60558-96-5) + [Cu(CH3CN)3](p-toluenesulfonate) (907562-32-7) → [(N,N,N',N'-tetraethylpropane-1,3-diamine)Cu(CH3CN)3](p-toluenesulfonate)

Guidance literature:

In dichloromethane; by mixing equimolar amts. of a ligand and Cu-contg. compd. in CH2Cl2;

DOI:10.1021/ja061132g

upstream raw materials:

tetra-N-ethyl-ξ-propenediyldiamine

diethylamine

1,3-dibromo-propane