3,3'-[1,2-Ethanediylbis(thio)]bis-1-propanol

Base Information

• Chemical Name: 3,3'-[1,2-Ethanediylbis(thio)]bis-1-propanol
• CAS No.: 4756-21-2
• Molecular Formula: C8H18 O2 S2
• Molecular Weight: 210.362
• Mol file: 4756-21-2.mol

Synonyms:1-Propanol,3,3'-(ethylenedithio)di- (6CI,7CI,8CI); 1,10-Dihydroxy-4,7-dithiadecane;4,7-Dithiadecane-1,10-diol

Chemical Property of 3,3'-[1,2-Ethanediylbis(thio)]bis-1-propanol

Chemical Property:

• PSA: 91.06000
• LogP: 1.21760

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,3'-[1,2-Ethanediylbis(thio)]bis-1-propanol

There total 4 articles about 3,3'-[1,2-Ethanediylbis(thio)]bis-1-propanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethylene dibromide (106-93-4) → 1,2-bis(3-hydroxypropylthio)ethane (4756-21-2)

Guidance literature:

With ethanol; zuletzt bei Siedetemperatur;

DOI:10.1080/10903120190939986

Reference yield:

ethane-1,2-dithiol (540-63-6) + 1-chloro-3-hydroxypropane (627-30-5) → 1,2-bis(3-hydroxypropylthio)ethane (4756-21-2)

Guidance literature:

With ethanol; sodium; Yield given. Multistep reaction; 1.) reflux, 2.) reflux, 2 h;

DOI:10.1016/S0022-328X(00)83008-9

Reference yield:

ethane-1,2-dithiol (540-63-6) + allyl alcohol (107-18-6) → 1,2-bis(3-hydroxypropylthio)ethane (4756-21-2)

Guidance literature:

With dibenzoyl peroxide; Irradiation_.im UV-Licht;

upstream raw materials:

ethane-1,2-dithiol

allyl alcohol

1-chloro-3-hydroxypropane

ethylene dibromide

Downstream raw materials:

4,7-dithiadecane-1,10-di-p-toluenesulfonate

Refernces