1-Octadecanesulfonyl chloride

Base Information

• Chemical Name: 1-Octadecanesulfonyl chloride
• CAS No.: 10147-41-8
• Molecular Formula: C18H37 Cl O2 S
• Molecular Weight: 353.01
• Hs Code.: 2904909090
• European Community (EC) Number: 233-417-3
• DSSTox Substance ID: DTXSID20143943
• Nikkaji Number: J227.071D
• Wikidata: Q83008004
• Mol file: 10147-41-8.mol

Synonyms:10147-41-8;1-OCTADECANESULFONYL CHLORIDE;octadecane-1-sulfonyl chloride;Octadecane-1-sulphonyl chloride;1-Octadecanesulphonyl chloride;EINECS 233-417-3;octadecanesulfonylchloride;octadecanesulfonyl chloride;C18H37ClO2S;SCHEMBL743460;C18-H37-Cl-O2-S;DTXSID20143943;MFCD00051521;AKOS016016482;1-Octadecanesulfonyl chloride AldrichCPR;1-Octadecanesulfonyl chloride, AldrichCPR;FT-0608172

Chemical Property of 1-Octadecanesulfonyl chloride

Chemical Property:

• Vapor Pressure: 3.24E-07mmHg at 25°C
• Melting Point: 58-60°C
• Boiling Point: 430.5°C at 760 mmHg
• Flash Point: 214.2°C
• PSA: 42.52000
• Density: 0.985g/cm³
• LogP: 7.89730
• Sensitive.: Moisture Sensitive
• XLogP3: 9.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 17
• Exact Mass: 352.2202793
• Heavy Atom Count: 22
• Complexity: 310

Purity/Quality:

98%,99%, ^*data from raw suppliers

1-OCTADECANESULFONYL CHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Statements: 34
• Safety Statements: 26-36/37/39-45

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCCCCCCCCCCCS(=O)(=O)Cl

Technology Process of 1-Octadecanesulfonyl chloride

There total 7 articles about 1-Octadecanesulfonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

Dithiocarbonic acid S,S-dioctadecyl ester (112096-11-4) → 1-octadecanesulfonyl chloride (10147-41-8)

Guidance literature:

With water; chlorine; at 5 - 10 ℃; for 1h;

DOI:10.1055/s-1989-27445

Reference yield:

octadecane-1-sulfonic acid (6140-87-0) → 1-octadecanesulfonyl chloride (10147-41-8)

Guidance literature:

With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; Heating / reflux;

Reference yield:

octadecane (593-45-3) → 1-octadecanesulfonyl chloride (10147-41-8)

Guidance literature:

With sulfuryl dichloride;

DOI:10.1007/s11743-010-1210-y

upstream raw materials:

S-octadecyl-isothiourea; hydrochloride

Dithiocarbonic acid S,S-dioctadecyl ester

octadecane-1-sulfonic acid

1-chlorooctadecane

Downstream raw materials:

1-chlorooctadecane

N-[(1R,2R)-2-(benzyloxy)cyclohexyl]octadecane-1-sulphonamide

N-[(1R,2R)-2-hydroxycyclohexyl]octadecane-1-sulphonamide

octadecanesulphonic acid sodium salt

Refernces

• 1、 Bougueroua,Mousli,Tazerouti. "Synthesis and Physicochemical Properties of Alanine-Based Surfactants". . p. 1121 - 1131. Retrieved 2016/10/18.
• 2、 -. "HETEROCYCLIC COMPOUNDS CONTAINING NITROGEN ATOMS OR PHARMACEUTICALLY ACCEPTABLE SALTS THEREOF, PROCESS FOR THE PREPARATION THEREOF AND PHARMACEUTICAL COMPOSITION COMPRISING THE SAME FOR TREATMENT OF CANCER". Page/Page column 14. . Retrieved 2010/06/19.