13H-Benzo[a]pyrido[3,2-i]carbazole

Base Information

• Chemical Name: 13H-Benzo[a]pyrido[3,2-i]carbazole
• CAS No.: 239-67-8
• Molecular Formula: C₁₉H₁₂N₂
• Molecular Weight: 268.318
• Hs Code.: 2933990090
• Mol file: 239-67-8.mol

Synonyms:7,8-Benzo-pyrido-(2',3':1,2)-carbazol;7,8-Benzopyrido(2',3':1,2)carbazole;7,8-Benzo-pyrido<3',2':1,2>carbazol;13H-Benzo(a)pyrido(3,2-i)carbazole;

Chemical Property of 13H-Benzo[a]pyrido[3,2-i]carbazole

Chemical Property:

• Vapor Pressure: 5.81E-12mmHg at 25°C
• Refractive Index: 1.8676 (estimate)
• Boiling Point: 559.2°Cat760mmHg
• Flash Point: 261.8°C
• PSA: 28.68000
• Density: 1.358g/cm³
• LogP: 5.02250

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 13H-Benzo[a]pyrido[3,2-i]carbazole

There total 1 articles about 13H-Benzo[a]pyrido[3,2-i]carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 13H-benzo[a]pyrido[3,2-i]carbazole (239-67-8)

Guidance literature:

α-Tetralon-, ZnCl2 (45 Min., 280 - 300grad);

Reference yield: 79.0%

{IrH2(acetone)2(PPh3)2}SbF6 (110077-68-4,89509-77-3) + 13H-benzo[a]pyrido[3,2-i]carbazole (239-67-8) → Ir(H)2(P(C6H5)3)2(C19H11N2)

Guidance literature:

In dichloromethane; N2-atmosphere; equimolar amts., room temp., stirring for 20 min; filtration (Celite), concn., pptn. on Et2O addn.; elem. anal.;

DOI:10.1021/ic00129a014