2-(p-Tolyloxy)ethyl acetate

Base Information

• Chemical Name: 2-(p-Tolyloxy)ethyl acetate
• CAS No.: 6807-11-0
• Molecular Formula: C11H14O3
• Molecular Weight: 194.23
• Hs Code.: 2915390090
• European Community (EC) Number: 229-881-1
• UNII: JE83E4XFCE
• DSSTox Substance ID: DTXSID90863949
• Nikkaji Number: J149.775H
• Wikidata: Q27281471
• Mol file: 6807-11-0.mol

Synonyms:2-(p-tolyloxy)ethyl acetate

Chemical Property of 2-(p-Tolyloxy)ethyl acetate

Chemical Property:

• Melting Point: 94 °C / 2mmHg
• Boiling Point: 266.9 °C at 760 mmHg
• Flash Point: 106.2 °C
• PSA: 35.53000
• Density: 1.063 g/cm³
• LogP: 1.93690
• XLogP3: 2.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 5
• Exact Mass: 194.094294304
• Heavy Atom Count: 14
• Complexity: 171

Purity/Quality:

98%,99%, ^*data from raw suppliers

4-(2-Acetoxyethoxy)toluene >98.0%(GC) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC=C(C=C1)OCCOC(=O)C

Technology Process of 2-(p-Tolyloxy)ethyl acetate

There total 2 articles about 2-(p-Tolyloxy)ethyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

2-(4-methylphenoxy)ethanol (15149-10-7) + acetic acid (64-19-7,77671-22-8) → 2-(p-tolyloxy)ethyl acetate (6807-11-0)

Guidance literature:

With nickel oxinate; In neat (no solvent); at 70 ℃;

DOI:10.1039/d0gc00520g

Reference yield:

→ 2-(p-tolyloxy)ethyl acetate (6807-11-0)

Guidance literature:

p-Kresol, Ethylenoxid, Essigsaeure;

Reference yield: 50.0%

2-(p-tolyloxy)ethyl acetate (6807-11-0) + para-bromoacetophenone (99-90-1) → C19H20O4

Guidance literature:

With nickel(II) bromide dimethoxyethane; 4,4'-Dimethoxy-2,2'-bipyridin; In tetrahydrofuran; acetonitrile; at 40 ℃; for 36h; Electrolysis;

DOI:10.1039/d0sc01445a

upstream raw materials:

2-(4-methylphenoxy)ethanol

acetic acid

Downstream raw materials:

2,2'-Methylen-bis-(5-methyl-1,2-phenylenoxy)-diethanol

Refernces