Hydroxyl amine iodide

Base Information

• Chemical Name: Hydroxyl amine iodide
• CAS No.: 59917-23-6
• Molecular Formula: H3NO•HI
• Molecular Weight: 160.942
• DSSTox Substance ID: DTXSID30208633
• Mol file: 59917-23-6.mol

Synonyms:Hydroxyl amine iodide;59917-23-6;Hydroxyl amine iodide [Forbidden];DTXSID30208633

Chemical Property of Hydroxyl amine iodide

Chemical Property:

• Vapor Pressure: 179mmHg at 25°C
• Boiling Point: 56.5°C at 760 mmHg
• Hydrogen Bond Donor Count: 3
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 0
• Exact Mass: 160.93376
• Heavy Atom Count: 3
• Complexity: 2

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: NO.I

Technology Process of Hydroxyl amine iodide

There total 3 articles about Hydroxyl amine iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

hydrogen iodide (10034-85-2) + hydroxylamine (7803-49-8) → hydroxylamine hydrogen iodide (59917-23-6)

Guidance literature:

In water; at 0 ℃; for 0.0833333h; pH=7;

DOI:10.1002/ejoc.201800304

Reference yield:

mercury(II) fulminate → hydroxylamine hydrogen iodide (59917-23-6)

Guidance literature:

With hydrogen iodide; byproducts: NH4I; fuming HI;

Reference yield:

hydroxyammonium sulfate + barium(II) iodide (13718-50-8) → hydroxylamine hydrogen iodide (59917-23-6)

Guidance literature:

In water; byproducts: barium sulfate; 1:1 stoich, ratio of BaI2:NH3OHSO4; filtered, filtrate evapd. in vac. at 0°C in the dark;

DOI:10.1039/F29817700287

upstream raw materials:

barium(II) iodide

hydrogen iodide

hydroxylamine

Downstream raw materials:

iodine

Refernces

• 1、 -. "METHOD FOR CLEAVING AMIDE BONDS". Paragraph 0072. . Retrieved 2019/01/25.