1-Chlorodibenzofuran

Base Information

• Chemical Name: 1-Chlorodibenzofuran
• CAS No.: 84761-86-4
• Molecular Formula: C₁₂H₇ClO
• Molecular Weight: 202.64
• UNII: 00SD1U3FL3
• DSSTox Substance ID: DTXSID701005060
• Nikkaji Number: J397.556H
• Wikidata: Q27231374
• Mol file: 84761-86-4.mol

Synonyms:1-CHLORODIBENZOFURAN;1-Chlorodibenzo[b,d]furan;84761-86-4;CCRIS 1437;Chlorodibenzofuran;Dibenzofuran, 1-chloro;UNII-00SD1U3FL3;00SD1U3FL3;PCDF 1;SCHEMBL472793;DTXSID701005060;MFCD00800057;SY277924;LS-188805;Q27231374

Chemical Property of 1-Chlorodibenzofuran

Chemical Property:

• Vapor Pressure: 0.000509mmHg at 25°C
• Boiling Point: 323°C at 760 mmHg
• Flash Point: 149.1°C
• PSA: 13.14000
• Density: 1.329g/cm³
• LogP: 4.23940
• XLogP3: 4.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 202.0185425
• Heavy Atom Count: 14
• Complexity: 218

Purity/Quality:

99% ^*data from raw suppliers

1-CHLORODIBENZOFURAN 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)C3=C(O2)C=CC=C3Cl

Technology Process of 1-Chlorodibenzofuran

There total 6 articles about 1-Chlorodibenzofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

2,3-diethynylbenzo[b]furan → 1-monochlorodibenzofuran (84761-86-4)

Guidance literature:

With hydrogenchloride; platinum(II) chloride; In water; at 100 ℃; for 9h;

DOI:10.1021/jo0518295

Reference yield: 9.0%

1-hydroxydibenzofuran (33483-06-6) → 1-monochlorodibenzofuran (84761-86-4)

Guidance literature:

With para-tert-butylphenol; phosphorus pentachloride; at 280 ℃; for 0.333333h;

Reference yield:

municipal waste → 3-chlorodibenzofuran (25074-67-3) + 1-monochlorodibenzofuran (84761-86-4) + 1,2,6-trichlorodibenzo-p-dioxin (82291-29-0) + 1,2,9-trichlorodibenzo-p-dioxin (82291-32-5)

Guidance literature:

With oxygen; at 350 ℃; Further byproducts given. Title compound not separated from byproducts; Formation of xenobiotics;

DOI:10.1016/S0045-6535(00)00223-X

upstream raw materials:

1-hydroxydibenzofuran

Pentachlorophenol

3-monochlorophenol

2,3,4-trichlorophenol

Refernces

• 1、 -. "COMPOUND FOR ORGANIC OPTOELECTRONIC DEVICE, COMPOSITION FOR ORGANIC OPTOELECTRONIC DEVICE, ORGANIC OPTOELECTRONIC DEVICE, AND DISPLAY DEVICE". Paragraph 0288; 0293-0294; 0304; 0307-0308. . Retrieved 2021/09/03.
• 2、 -. "COMPOSITION AND ORGANIC OPTOELECTRONIC DEVICE AND DISPLAY DEVICE". Paragraph 0331-0332; 0337-0338; 0348-0349; 0352-0353. . Retrieved 2020/02/19.