1-METHYLFLUORANTHENE

Base Information

• Chemical Name: 1-METHYLFLUORANTHENE
• CAS No.: 25889-60-5
• Molecular Formula: C₁₇H₁₂
• Molecular Weight: 216.282
• Hs Code.: 2902909090
• Mol file: 25889-60-5.mol

Synonyms:1-Methylfluoranthene

Chemical Property of 1-METHYLFLUORANTHENE

Chemical Property:

• Vapor Pressure: 7.38E-06mmHg at 25°C
• Melting Point: 74-76 °C
• Boiling Point: 387.4°C at 760 mmHg
• Flash Point: 178.9°C
• PSA: 0.00000
• Density: 1.213g/cm³
• LogP: 4.79560

Purity/Quality:

98% ^*data from raw suppliers

1-Methylfluoranthene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-METHYLFLUORANTHENE

There total 14 articles about 1-METHYLFLUORANTHENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-hydroxy-4-methylcyclohexanone (118759-44-7,39512-01-1) → 1-methylfluoranthene (25889-60-5)

Guidance literature:

Multi-step reaction with 4 steps

1: KOH / methanol

2: H₂ / Raney-Ni

3: polyphosphoric acid

4: sulfur / 220 °C

With potassium hydroxide; PPA; hydrogen; sulfur; nickel; In methanol;

Reference yield:

(E)-benzalacetone (1896-62-4) → 1-methylfluoranthene (25889-60-5)

Guidance literature:

Multi-step reaction with 4 steps

1: KOH / methanol

2: H₂ / Raney-Ni

3: polyphosphoric acid

4: sulfur / 220 °C

With potassium hydroxide; PPA; hydrogen; sulfur; nickel; In methanol;

Reference yield:

7-Methyl-1-phenyl-Δ2-3,9-1-hexalin (93872-50-5) → 1-methylfluoranthene (25889-60-5)

Guidance literature:

With sulfur; at 220 ℃;

upstream raw materials:

1-methyl-1,2,3,10b-tetrahydro-fluoranthene

tetrachloromethane

chloranil

7-Methyl-1-phenyl-Δ^2-3,9-1-hexalin

Refernces

• 1、 Peake, D. A.,Oyler, A. R.,Heikkila, K. E.,Liukkonen, R. J.,Engroff, E. C.,Carlson, R. M.. "ALKYL AROMATIC SYNTHESIS: NUCLEOPHILIC ALKYL LITHIUM ADDITION". . p. 21 - 26. Retrieved 2007/10/02.