2,2'-Diaminobenzophenone

Base Information

• Chemical Name: 2,2'-Diaminobenzophenone
• CAS No.: 606-10-0
• Molecular Formula: C13H12 N2 O
• Molecular Weight: 212.251
• Mol file: 606-10-0.mol

Synonyms:Benzophenone,2,2'-diamino- (7CI,8CI); 2,2'-Diaminobenzophenone; o,o'-Diaminobenzophenone

Chemical Property of 2,2'-Diaminobenzophenone

Chemical Property:

• Boiling Point: 469.4 °C at 760 mmHg
• Flash Point: 237.7 °C
• PSA: 69.11000
• Density: 1.233 g/cm³
• LogP: 3.24440

Purity/Quality:

98%min ^*data from raw suppliers

2,2'-DIAMINOBENZOPHENONE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,2'-Diaminobenzophenone

There total 7 articles about 2,2'-Diaminobenzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

2-iodophenylamine (615-43-0) → 2,2'-diaminobenzophenone (606-10-0)

Guidance literature:

With (2,2'-bipyridine)nickel(II) dibromide; tetrabutylammonium tetrafluoroborate; In N,N-dimethyl-formamide; Ambient temperature; electrolysis;

DOI:10.1016/S0040-4020(97)10143-0

Reference yield:

2,2'-dinitro-benzophenone (51727-42-5) → 2,2'-diaminobenzophenone (606-10-0) + 10H-acridin-9-one (578-95-0,790240-54-9)

Guidance literature:

In ethanol; Product distribution; Mechanism; electrochemical reduction at mercury electrodes;

Reference yield:

2,2'-dinitro-benzophenone (51727-42-5) → 2,2'-diaminobenzophenone (606-10-0)

Guidance literature:

With hydrogenchloride; tin;

upstream raw materials:

2,2'-dinitro-benzophenone

2-iodophenylamine

phenyl (3-amino-4-nitrophenyl)-methanone

Downstream raw materials:

2,2'-bis-acetylamino-benzophenone

acridine

o,o'-diiodobenzophenone

10H-acridin-9-one

Refernces

• 1、 Dolhem,Ocafrain,Nedelec,Troupel. "Nickel catalyzed electrosynthesis of ketones from organic halides and metal carbonyls". . p. 17089 - 17096. Retrieved 2007/10/03.
• 2、 Voigtlaender, Rolf,Hlavaty, Jaromir,Volke, Jiri,Bakos, Viktor. "ELECTROCHEMICAL REDUCTION OF 2,2'-DINITRODIPHENYLMETHANE AND 2,2'-DINITROBENZOPHENONE AT MERCURY ELECTRODES". . p. 364 - 378. Retrieved 2007/10/02.