3'-Methylpropiophenone

Base Information Edit

Chemical Name:3'-Methylpropiophenone
CAS No.:51772-30-6
Molecular Formula:C10H12O
Molecular Weight:148.205
Hs Code.:2914399090
European Community (EC) Number:257-405-2
UNII:MRV2PZ9ZV1
DSSTox Substance ID:DTXSID90199699
Nikkaji Number:J294.904K
Wikidata:Q27284200
Mol file:51772-30-6.mol

Synonyms:3'-Methylpropiophenone;51772-30-6;1-(3-methylphenyl)propan-1-one;m-METHYLPROPIOPHENONE;1-(m-Tolyl)propan-1-one;1-Propanone, 1-(3-methylphenyl)-;1-(3-Methylphenyl)-1-propanone;UNII-MRV2PZ9ZV1;MRV2PZ9ZV1;EINECS 257-405-2;MFCD00027014;m-n-propoyltoluene;3`-Methylpropiophenone;1-m-tolylpropan-1-one;1-m-Tolyl-propan-1-one;SCHEMBL634002;AMY8744;DTXSID90199699;BCA77230;AKOS010015354;CS-11054;SY004012;A7618;CS-0186845;FT-0640024;1-(3-Methylphenyl)-1-propanone, AldrichCPR;EN300-210282;3 inverted exclamation mark -Methylpropiophenone;Q27284200

Suppliers and Price of 3'-Methylpropiophenone

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 84 raw suppliers

Chemical Property of 3'-Methylpropiophenone Edit

Chemical Property:

Melting Point:-4.4°C
Refractive Index:1.5413 (estimate)
Boiling Point:230.3 °C at 760 mmHg
Flash Point:98.1 °C
PSA：17.07000
Density:0.963 g/cm³
LogP:2.58770
Storage Temp.:Refrigerator, Under inert atmosphere
Solubility.:Chloroform (Soluble), Methanol (Sparingly)
XLogP3:2.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:148.088815002
Heavy Atom Count:11
Complexity:140

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC(=O)C1=CC=CC(=C1)C

Technology Process of 3'-Methylpropiophenone

There total 23 articles about 3'-Methylpropiophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 925-90-6
ethylmagnesium bromide

: 620-22-4
3-Methylbenzonitrile

: 51772-30-6
3'-Methylpropiophenone

Guidance literature:: ethylmagnesium bromide; 3-Methylbenzonitrile; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

With water; In tetrahydrofuran; Cooling with ice;
DOI:10.1021/jm901189z

Reference yield: 90.0%

: 67-56-1
methanol

: 7287-81-2,25675-28-9,42070-91-7,51154-53-1
1-(m-methylphenyl)ethanol

: 51772-30-6
3'-Methylpropiophenone

Guidance literature:: With chlorine[2-(4,5-dihydro-1H-imidazol-2-yl)-6-methoxypyridine](pentamethylcyclopentadienyl)iridium(III) chloride; potassium hydroxide; In water; at 80 ℃; for 18h; chemoselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1002/ejoc.202001550

Reference yield: 88.0%

: 74-85-1
ethene

: 99-04-7
m-Toluic acid

: 51772-30-6
3'-Methylpropiophenone

Guidance literature:: With (1,2-dimethoxyethane)dichloronickel(II); 5, 6-dimethyl-1,10-phenanthroline; [4,4′-bis(1,1-dimethylethyl)-2,2′-bipyridine-N1,N1′]bis{3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-κN]phenyl-κC}iridium(III) hexafluorophosphate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In acetonitrile; at 20 ℃; for 2h; under 760.051 Torr; Irradiation; Inert atmosphere; Sealed tube; Schlenk technique;
DOI:10.1039/d1cc04188f