octyl carbamimidothioate

Base Information

• Chemical Name: octyl carbamimidothioate
• CAS No.: 4270-03-5
• Molecular Formula: C9H20 N2 S . Br H
• Molecular Weight: 269.249
• Mol file: 4270-03-5.mol

Synonyms:Pseudourea,2-octyl-2-thio-, hydrobromide (7CI,8CI);S-Octylisothiouronium bromide;S-Octylisothiuronium bromide;

Chemical Property of octyl carbamimidothioate

Chemical Property:

• Vapor Pressure: 0.00496mmHg at 25°C
• Refractive Index: 1.512
• Boiling Point: 275.9°Cat760mmHg
• Flash Point: 120.6°C
• Density: 1.02g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of octyl carbamimidothioate

There total 1 articles about octyl carbamimidothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1-bromo-octane (111-83-1) + thiourea (17356-08-0) → 2-n-octylisothiourea hydrobromide (4270-03-5)

Guidance literature:

In ethanol; Reflux;

DOI:10.1080/00397911.2018.1557687

Reference yield: 95.0%

2-n-octylisothiourea hydrobromide (4270-03-5) → octane-1-sulfonyl chloride (7795-95-1)

Guidance literature:

With tert-butylhypochlorite; In water; acetonitrile; at 0 - 20 ℃;

DOI:10.1055/s-0034-1381024

Reference yield: 70.0%

Benzylidenemalononitrile (2700-22-3) + 2-n-octylisothiourea hydrobromide (4270-03-5) → 4-amino-2-(octylthio)-6-phenylpyrimidine-5-carbonitrile

Guidance literature:

With potassium carbonate; In isopropyl alcohol; Reflux;

DOI:10.1080/00397911.2018.1557687

upstream raw materials:

1-bromo-octane

thiourea

Downstream raw materials:

3-(octylthio)propanoic acid

octane-1-sulfonyl chloride

Refernces

• 1、 Qiu, Kui,Wang, Rennan. "Tert -Butyl Hypochlorite Mediated Oxidative Chlorination of S -Alkylisothiourea Salts: Synthesis of Sulfonyl Chlorides". . p. 3186 - 3190. Retrieved 2015/10/19.
• 2、 Sabirov, S. S.,Gnevasheva, L. M.,Ismailov, M. I.,Isobaev, M. D.. "SYNTHESIS OF MONO(ALKYLTHIO)-SUBSTITUTED KETONES". . p. 1239 - 1243. Retrieved 2007/10/02.