4-Benzyloxy-3-methoxy-beta-nitrostyrene

Base Information Edit

Chemical Name:4-Benzyloxy-3-methoxy-beta-nitrostyrene
CAS No.:1860-56-6
Molecular Formula:C₁₆H₁₅NO₄
Molecular Weight:285.299
Hs Code.:
European Community (EC) Number:631-591-9
Nikkaji Number:J1.401.185D
Wikidata:Q106902746
ChEMBL ID:CHEMBL594878
Mol file:1860-56-6.mol

Synonyms:63909-38-6;4-Benzyloxy-3-methoxy-beta-nitrostyrene;(E)-1-(benzyloxy)-2-methoxy-4-(2-nitrovinyl)benzene;4-Benzyloxy-3-methoxy-omega-nitrostyrene;1860-56-6;1-(benzyloxy)-2-methoxy-4-[(E)-2-nitroethenyl]benzene;2-methoxy-4-[(E)-2-nitroethenyl]-1-phenylmethoxybenzene;1-(Benzyloxy)-2-methoxy-4-(2-nitrovinyl)benzene;NSC 22600;ANISOLE, 2-(BENZYLOXY)-5-(2-NITROVINYL)-;4-Benzyloxy-3-methoxy-|A-nitrostyrene;Benzene, 2-methoxy-4-(2-nitroethenyl)-1-(phenylmethoxy)-;1-(benzyloxy)-2-methoxy-4-[(1E)-2-nitroethenyl]benzene;CHEMBL594878;SCHEMBL4903808;SCHEMBL5185813;ANM100092;4-Benzyloxy-3-methoxy-?-nitrostyrene;AKOS002957702;AT12763;4-Benzyloxy-3-methoxy-.beta.-nitrostyrene;trans-4-Benzyloxy-3-methoxy-beta-nitrostyrene;trans-4-benzyloxy-3-methoxy-beta-nitro-styrene;Styrene, 4-(benzyloxy)-3-methoxy-.beta.-nitro-

Suppliers and Price of 4-Benzyloxy-3-methoxy-beta-nitrostyrene

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
4-Benzyloxy-3-methoxy-β-nitrostyrene
10g
$ 1100.00

Sigma-Aldrich
1-(BENZYLOXY)-2-METHOXY-4-[(E)-2-NITROETHENYL]BENZENE Aldrich
1ea
$ 144.00

Biosynth Carbosynth
1-(4-Benzyloxy-3-methoxyphenyl)-2-nitroethene
10 g
$ 125.00

Biosynth Carbosynth
1-(4-Benzyloxy-3-methoxyphenyl)-2-nitroethene
5 g
$ 75.00

Biosynth Carbosynth
1-(4-Benzyloxy-3-methoxyphenyl)-2-nitroethene
25 g
$ 250.00

American Custom Chemicals Corporation
2-METHOXY-4-[(Z)-2-NITROETHENYL]-1-PHENYLMETHOXYBENZENE 95.00%
5MG
$ 499.10

AK Scientific
4-Benzyloxy-3-methoxy-beta-nitrostyrene
5g
$ 151.00

AHH
4-Benzyloxy-3-methoxy-omega-nitrostyrene 99%
25g
$ 330.00

Total 9 raw suppliers

Chemical Property of 4-Benzyloxy-3-methoxy-beta-nitrostyrene Edit

Chemical Property:

Vapor Pressure:6.99E-08mmHg at 25°C
Melting Point:122-124?°C(lit.)
Boiling Point:450.5°C at 760 mmHg
Flash Point:191.8°C
PSA：64.28000
Density:1.212g/cm³
LogP:4.04480
Solubility.:Acetic Acid, Dichloromethane, Ethyl Acetate, Methanol
XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:285.10010796
Heavy Atom Count:21
Complexity:347

Purity/Quality:

98%,99%, ^*data from raw suppliers

4-Benzyloxy-3-methoxy-β-nitrostyrene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xi
Statements: 36/37/38
Safety Statements: 26-36

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=CC(=C1)C=C[N+](=O)[O-])OCC2=CC=CC=C2
Isomeric SMILES:COC1=C(C=CC(=C1)/C=C/[N+](=O)[O-])OCC2=CC=CC=C2

Technology Process of 4-Benzyloxy-3-methoxy-beta-nitrostyrene

There total 18 articles about 4-Benzyloxy-3-methoxy-beta-nitrostyrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.8%

: 2426-87-1
3-methoxy-4-(phenylmethoxy)benzaldehyde

: 75-52-5
nitromethane

: 63909-38-6,1860-56-6
3-methoxy-4-benzyloxy-ω-nitrostyrolene

Guidance literature:: With ammonium acetate; at 80 ℃; for 1.5h;

Reference yield: 85.0%

: 60372-07-8
1-(3-methoxy-4-benzyloxyphenyl)-2-nitroethanol

: 63909-38-6,1860-56-6
3-methoxy-4-benzyloxy-ω-nitrostyrolene

Guidance literature:: With sodium acetate; acetic anhydride; for 0.0833333h; Heating;

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 63909-38-6,1860-56-6
3-methoxy-4-benzyloxy-ω-nitrostyrolene

Guidance literature:: Multi-step reaction with 2 steps

1: KOH / ethanol / Heating

2: NH₄OAc / acetic acid / Heating

With potassium hydroxide; ammonium acetate; In ethanol; acetic acid;