1-Aminononadecane

Base Information

• Chemical Name: 1-Aminononadecane
• CAS No.: 14130-05-3
• Deprecated CAS: 84778-43-8
• Molecular Formula: C19H41N
• Molecular Weight: 283.541
• Hs Code.: 2921199090
• European Community (EC) Number: 268-215-4,672-723-5
• DSSTox Substance ID: DTXSID00867438
• Nikkaji Number: J151.194G
• Mol file: 14130-05-3.mol

Synonyms:1-Aminononadecane;14130-05-3;nonadecan-1-amine;Nonadecylamine;1-Nonadecanamine;n-Nonadecylamine;68037-92-3;EINECS 268-215-4;1-Nonadecanamine #;EC 268-215-4;SCHEMBL157850;DTXSID00867438;MFCD00047944;L(-)-ARABONICACID-GAMMA-LACTONE;A0765;CS-0445978;FT-0637015;T70261;A807748

Chemical Property of 1-Aminononadecane

Chemical Property:

• Vapor Pressure: 2.07E-05mmHg at 25°C
• Melting Point: 53 °C
• Refractive Index: 1.453
• Boiling Point: 361.4 °C at 760 mmHg
• PKA: 10.67±0.10(Predicted)
• Flash Point: 161.5 °C
• PSA: 26.02000
• Density: 0.819g/cm³
• LogP: 7.29700
• Storage Temp.: 0-10°C
• Solubility.: almost transparency in hot Methanol
• XLogP3: 9.1
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 17
• Exact Mass: 283.323900312
• Heavy Atom Count: 20
• Complexity: 156

Purity/Quality:

98%,99%, ^*data from raw suppliers

1-Aminononadecane ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Chemical Classes: UVCB
• Canonical SMILES: CCCCCCCCCCCCCCCCCCCN

Technology Process of 1-Aminononadecane

There total 13 articles about 1-Aminononadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

N-nonadecyl nitrile (28623-46-3) → 1-nonadecanamine (n-nonadecylamine) (14130-05-3)

Guidance literature:

With ammonia; hydrogen; In water; isopropyl alcohol; at 80 ℃; for 24h; under 15001.5 Torr; Autoclave;

DOI:10.1002/chem.202001866

Reference yield: 35.0%

N-nonadecyl nitrile (28623-46-3) → octadecane (593-45-3) + 1-nonadecanamine (n-nonadecylamine) (14130-05-3)

Guidance literature:

With potassium; isopropyl alcohol; perhydrodibenzo-18-crown-6; In tetrahydrofuran; Ambient temperature;

DOI:10.1016/S0040-4039(00)95137-2

Reference yield:

17-hydroxyimino-hexatriacontanoic acid + sulfuric acid (7664-93-9) → 1-nonadecanamine (n-nonadecylamine) (14130-05-3) + Arachidic acid (506-30-9) + heptadecanedioic acid (2424-90-0)

Guidance literature:

Erhitzen des Reaktionsprodukts mit konz. HCl auf 180grad;

upstream raw materials:

Eicosanylamide

nonacosan-10-one oxime

N-nonadecyl nitrile

sulfuric acid

Downstream raw materials:

(2-benzyloxy-1-nonadecylcarbamoyl-ethyl)-carbamic acid tert-butyl ester

2-amino-3-benzyloxy-N-nonadecyl-propionamide

Octadecanoic acid ((S)-2-benzyloxy-1-nonadecylcarbamoyl-ethyl)-amide

Refernces

• 1、 Ohsawa, Tomihiko,Kobayashi, Takao,Mizuguchi, Yuko. "DISSOLVING METAL REDUCTION WITH CROWN ETHER----- REDUCTIVE DECYANATION". . p. 6103 - 6106. Retrieved 2007/10/02.