ethyl 3-hydroxytridecanoate

Base Information

• Chemical Name: ethyl 3-hydroxytridecanoate
• CAS No.: 107141-15-1
• Molecular Formula: C15H30O3
• Molecular Weight: 258.39700
• Mol file: 107141-15-1.mol

Synonyms:3-Hydroxy-tridecansaeure-aethylester;Tridecanoic acid,3-hydroxy-,ethyl ester;3-hydroxy-tridecanoic acid ethyl ester;

Chemical Property of ethyl 3-hydroxytridecanoate

Chemical Property:

• Vapor Pressure: 1.33E-06mmHg at 25°C
• Boiling Point: 359.1oC at 760 mmHg
• Flash Point: 137.5oC
• PSA: 46.53000
• Density: 0.931g/cm3
• LogP: 3.83130

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ethyl 3-hydroxytridecanoate

There total 3 articles about ethyl 3-hydroxytridecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

Decyl-oxiran (2855-19-8) + ethanol (64-17-5) + carbon monoxide (201230-82-2) → 3-hydroxytridecanoic acid ethyl ester (107141-15-1)

Guidance literature:

With NH-pyrazole; manganese; cobalt(II) bromide; at 60 ℃; for 20h; under 30003 Torr; Autoclave; Sealed tube; Inert atmosphere;

DOI:10.1021/acs.joc.9b01007

Reference yield:

ethyl 3-oxotridecanoate (74631-91-7) → 3-hydroxytridecanoic acid ethyl ester (107141-15-1)

Guidance literature:

With diethyl ether; aluminium amalgam;

Reference yield:

undecanoyl chloride (17746-05-3) → 3-hydroxytridecanoic acid ethyl ester (107141-15-1)

Guidance literature:

Multi-step reaction with 2 steps

1: Erwaermen des nach dem Ansaeuern erhaltenen Reaktionsprodukts mit Essigsaeure und wenig Schwefelsaeure

2: amalgamated aluminium; water containing diethyl ether

With diethyl ether; aluminium amalgam;

upstream raw materials:

ethyl 3-oxotridecanoate

undecanoyl chloride

Decyl-oxiran

ethanol

Refernces