tris(trifluoromethyl)stibane

Base Information

• Chemical Name: tris(trifluoromethyl)stibane
• CAS No.: 432-05-3
• Molecular Formula: C3F9Sb
• Molecular Weight: 328.769
• Mol file: 432-05-3.mol

Synonyms:

Chemical Property of tris(trifluoromethyl)stibane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of tris(trifluoromethyl)stibane

There total 6 articles about tris(trifluoromethyl)stibane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

antimony (7440-36-0) + iodotrifluoromethane (2314-97-8,263005-66-9) → tris(trifluoromethyl)stibane (432-05-3) + Bis(trifluormethyl)-jodstiban (1479-46-5) + antimony triiodide (7790-44-5)

Guidance literature:

various ratios of Sb and CF3I (100:75 to 50:110), in rotating steelcylinder, 165 to 170°C, 50 atm; distn.;

DOI:10.1039/JR9570003708

Reference yield: 63.0%

bis(trifluoromethyl)mercury (371-76-6) + antimony triiodide (7790-44-5) → iodotrifluoromethane (2314-97-8,263005-66-9) + tris(trifluoromethyl)stibane (432-05-3) + Bis(trifluormethyl)-jodstiban (1479-46-5)

Guidance literature:

SbI3 and Hg(CF3)2 heated to 165°C for 8h; at -131°C sepd. (CF3)2SbI and Sb(CF3)3;

Reference yield:

Bis(trifluormethyl)-chlorstiban (650-53-3) → tris(trifluoromethyl)stibane (432-05-3) + antimony(III) chloride (10025-91-9)

Guidance literature:

distn.;

DOI:10.1039/JR9570003708

upstream raw materials:

Bis(trifluormethyl)-chlorstiban

antimony

iodotrifluoromethane

bis(trifluoromethyl)mercury

Downstream raw materials:

Carbonyl fluoride

2-(trifluoromethyl)furan

trifluoromethan

2,3-Dihydro-2-trifluormethylfuran

Refernces