Technology Process of Propanedioic acid,
[2-[3-[2-[(phenylsulfonyl)methyl]phenyl]propyl]cyclopentyl]-, dimethyl
ester, cis-
There total 7 articles about Propanedioic acid,
[2-[3-[2-[(phenylsulfonyl)methyl]phenyl]propyl]cyclopentyl]-, dimethyl
ester, cis- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
perchloric acid; hydrogen;
platinum on activated charcoal;
In
methanol;
for 13h;
under 38786.1 Torr;
DOI:10.1021/jo00244a015
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 2.) H2O / 1.) toluene, reflux, 18 h, 2.) reflux, 30 min
2: TiCl4, CCl4, pyridine / tetrahydrofuran / 18 h / 25 °C
3: 89 percent / H2, 70percent HClO4 / 5percent Pt/C / methanol / 13 h / 38786.1 Torr
With
pyridine; tetrachloromethane; perchloric acid; water; hydrogen; titanium tetrachloride;
platinum on activated charcoal;
In
tetrahydrofuran; methanol;
DOI:10.1021/jo00244a015
- Guidance literature:
-
Multi-step reaction with 5 steps
1: triethylamine / CH2Cl2 / 3 h / 0 °C
2: NaI / acetone / 2 h / Heating
3: 2.) H2O / 1.) toluene, reflux, 18 h, 2.) reflux, 30 min
4: TiCl4, CCl4, pyridine / tetrahydrofuran / 18 h / 25 °C
5: 89 percent / H2, 70percent HClO4 / 5percent Pt/C / methanol / 13 h / 38786.1 Torr
With
pyridine; tetrachloromethane; perchloric acid; water; hydrogen; titanium tetrachloride; triethylamine; sodium iodide;
platinum on activated charcoal;
In
tetrahydrofuran; methanol; dichloromethane; acetone;
DOI:10.1021/jo00244a015