Technology Process of 3,4-Dimethoxybenzenethiolate
There total 8 articles about 3,4-Dimethoxybenzenethiolate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium hydroxide;
In
methanol;
for 2h;
Reflux;
- Guidance literature:
-
C11H14O3S2;
With
potassium hydroxide;
In
ethanol;
at 80 ℃;
for 16h;
With
hydrogenchloride;
In
water;
pH=1;
With
lithium aluminium tetrahydride;
In
diethyl ether;
at 0 - 25 ℃;
for 2h;
Inert atmosphere;
DOI:10.1021/acs.macromol.6b00629
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: NaH / dimethylformamide
1.2: 47 percent / dimethylformamide / Heating
2.1: 100 percent / 6 h / 285 °C
3.1: 99 percent / KOH / methanol / Heating
With
potassium hydroxide; sodium hydride;
In
methanol; N,N-dimethyl-formamide;
2.1: Newman-Kwart rearrangement;
DOI:10.1021/jm0493109
