Technology Process of Decanoic acid, 2-methyl-, ethyl ester
There total 1 articles about Decanoic acid, 2-methyl-, ethyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
titanium(IV) isopropylate; lithium chloride; palladium dichloride; 1,3,5,7-tetramethyl-8-phenyl-2,4,6-trioxa-8-phosphatricyclo[3.3.1.13,7]decane;
In
1,2-dimethoxyethane;
at 110 ℃;
for 22h;
under 18100.7 Torr;
Overall yield = 67 %; regioselective reaction;
Autoclave;
DOI:10.1021/acs.joc.5b00851
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
at 0 ℃;
for 0.75h;
DOI:10.1021/ol0626140