4-([6-(3-BUTENOYLOXY)HEXYL]OXY)BENZENECARBOXYLIC ACID

Base Information

• Chemical Name: 4-([6-(3-BUTENOYLOXY)HEXYL]OXY)BENZENECARBOXYLIC ACID
• CAS No.: 141522-65-8
• Molecular Formula: C₁₇H₂₂O₅
• Molecular Weight: 306.359
• Mol file: 141522-65-8.mol

Synonyms:4-[6-(but-3-enoyloxy)hexyloxy]benzoic acid;4-(6-But-3-enoyloxy-hexyloxy)-benzoic acid;

Chemical Property of 4-([6-(3-BUTENOYLOXY)HEXYL]OXY)BENZENECARBOXYLIC ACID

Chemical Property:

• PSA: 72.83000
• LogP: 3.44330

Purity/Quality:

4-{[6-(3-Butenoyloxy)hexyl]oxy}benzenecarboxylic acid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-([6-(3-BUTENOYLOXY)HEXYL]OXY)BENZENECARBOXYLIC ACID

There total 3 articles about 4-([6-(3-BUTENOYLOXY)HEXYL]OXY)BENZENECARBOXYLIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

but-3-enoic acid (625-38-7) + 4-(6-hydroxyhexyloxy)benzoic acid (83883-25-4) → 4-<6-(but-3-enoyloxy)hexyloxy>benzoic acid (141522-65-8)

Guidance literature:

With toluene-4-sulfonic acid; hydroquinone;

Reference yield:

1-bromo-6-hexanol (4286-55-9) → 4-<6-(but-3-enoyloxy)hexyloxy>benzoic acid (141522-65-8)

Guidance literature:

Multi-step reaction with 2 steps

1: KOH, KI / ethanol; H₂O

2: 86 percent / p-TsOH, benzene-1,4-diol

With potassium hydroxide; toluene-4-sulfonic acid; hydroquinone; potassium iodide; In ethanol; water;

Reference yield:

4-hydroxy-benzoic acid (99-96-7) → 4-<6-(but-3-enoyloxy)hexyloxy>benzoic acid (141522-65-8)

Guidance literature:

Multi-step reaction with 2 steps

1: KOH, KI / ethanol; H₂O

2: 86 percent / p-TsOH, benzene-1,4-diol

With potassium hydroxide; toluene-4-sulfonic acid; hydroquinone; potassium iodide; In ethanol; water;

upstream raw materials:

but-3-enoic acid

4-(6-hydroxyhexyloxy)benzoic acid

1-bromo-6-hexanol

4-hydroxy-benzoic acid

Downstream raw materials:

4-cyanophenyl 4-<6-(but-3-enoyloxy)hexyloxy>benzoate

4-cyano-3-fluorophenyl 4-<6-(but-3-enoyloxy)hexyloxy>benzoate

Refernces