Technology Process of D-lyxo-Hexose, 2-deoxy-
There total 17 articles about D-lyxo-Hexose, 2-deoxy- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 78 percent / potassium tert-butoxide / tetrahydrofuran; dimethylsulfoxide / 0.75 h / 23 °C
2: 77 percent / LiAlH4 / tetrahydrofuran / 3 h
3: 84 percent / pyridine / 4 °C
4: 77 percent / HgO, BF3*Et2O / 0.5 h
5: 94 percent / 0.2 M NaOMe / methanol / 16 h / 4 °C
6: 83 percent / 0.01 M trifluoroacetic acid / 24 h / 4 °C
With
lithium aluminium tetrahydride; boron trifluoride diethyl etherate; potassium tert-butylate; sodium methylate; trifluoroacetic acid; mercury(II) oxide;
In
tetrahydrofuran; pyridine; methanol; dimethyl sulfoxide;
DOI:10.1016/S0008-6215(00)85317-3
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 84 percent / pyridine / 4 °C
2: 77 percent / HgO, BF3*Et2O / 0.5 h
3: 94 percent / 0.2 M NaOMe / methanol / 16 h / 4 °C
4: 83 percent / 0.01 M trifluoroacetic acid / 24 h / 4 °C
With
boron trifluoride diethyl etherate; sodium methylate; trifluoroacetic acid; mercury(II) oxide;
In
pyridine; methanol;
DOI:10.1016/S0008-6215(00)85317-3
