Technology Process of Benzoic acid, 3,3'-methylenebis[4,6-dimethoxy-2,5-dimethyl-
There total 8 articles about Benzoic acid, 3,3'-methylenebis[4,6-dimethoxy-2,5-dimethyl- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium hydroxide;
In
dimethyl sulfoxide;
DOI:10.1021/jm960437a
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 100 percent / BF3*OEt2 / toluene / 0.25 h / Ambient temperature
2: 2.97 g / K2CO3 / acetone / Heating
3: 95 percent / aq. KOH / dimethylsulfoxide
With
potassium hydroxide; boron trifluoride diethyl etherate; potassium carbonate;
In
dimethyl sulfoxide; acetone; toluene;
DOI:10.1021/jm960437a
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 6.8 g / K2CO3 / acetone / 2 h / Heating
2: 3.18 g / NaBH4 / propan-2-ol
3: 3.35 g / pyridine, (dimethylamino)pyridine / CH2Cl2 / 2 h / Ambient temperature
4: 100 percent / BF3*OEt2 / toluene / 0.25 h / Ambient temperature
5: 2.97 g / K2CO3 / acetone / Heating
6: 95 percent / aq. KOH / dimethylsulfoxide
With
pyridine; dmap; potassium hydroxide; sodium tetrahydroborate; boron trifluoride diethyl etherate; potassium carbonate;
In
dichloromethane; dimethyl sulfoxide; isopropyl alcohol; acetone; toluene;
DOI:10.1021/jm960437a