N,2,2,2-tetrachloroacetamide

Base Information

• Chemical Name: N,2,2,2-tetrachloroacetamide
• CAS No.: 35077-10-2
• Molecular Formula: C2HCl4NO
• Molecular Weight: 196.848
• Mol file: 35077-10-2.mol

Synonyms:N,2,2,2-Tetrachloroacetamide;N-Chlorotrichloroacetamide;

Chemical Property of N,2,2,2-tetrachloroacetamide

Chemical Property:

• Refractive Index: 1.518
• Density: 1.74 g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N,2,2,2-tetrachloroacetamide

There total 2 articles about N,2,2,2-tetrachloroacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

dichloroacetamide (683-72-7) → N-chloro-trichloroacetamide (35077-10-2) + N-chloro-2,2-dichloroacetamide (35077-09-9)

Guidance literature:

With tert-butylhypochlorite; In ethanol;

Reference yield:

trichloroacetamide (594-65-0) → N-chloro-trichloroacetamide (35077-10-2)

Guidance literature:

With water; chlorine;

Reference yield: 70.0%

N-chloro-trichloroacetamide (35077-10-2) + 4-chloro-benzenesulfenyl chloride (933-01-7) → C8H4Cl5NOS (81386-76-7)

Guidance literature:

With pyridine; In benzene; at 20 ℃; for 2h; further base;

upstream raw materials:

trichloroacetamide

dichloroacetamide

Downstream raw materials:

C₈H₆Cl₅NOSe

(+/-)-C_.C_.C-trichloro-N-(trans-2-chloro-cyclohexyl)-acetamide

2,2,2-Trichloro-N-((1R,2S)-2-chloro-cyclohexyl)-acetamide

trichloroacetamide

Refernces

• 1、 -. "N-chloro-chloroacetamides as herbicides". . . Retrieved 2008/06/13.