9-oxo-9H-fluorene-2-carbonitrile

Base Information

• Chemical Name: 9-oxo-9H-fluorene-2-carbonitrile
• CAS No.: 3096-44-4
• Molecular Formula: C14H7 N O
• Molecular Weight: 205.216
• Mol file: 3096-44-4.mol

Synonyms:Fluorene-2-carbonitrile,9-oxo- (6CI,7CI,8CI); NSC 74977

Chemical Property of 9-oxo-9H-fluorene-2-carbonitrile

Chemical Property:

• Vapor Pressure: 8.52E-07mmHg at 25°C
• Boiling Point: 405.8°Cat760mmHg
• Flash Point: 199.2°C
• Density: 1.33g/cm³

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 9-oxo-9H-fluorene-2-carbonitrile

There total 1 articles about 9-oxo-9H-fluorene-2-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-iodo-9H-fluorene (2523-42-4) → 9H-fluorene-9-oxo-2-carbossamide (3096-44-4)

Guidance literature:

Multi-step reaction with 2 steps

2: CuCN / dimethylformamide

With CuCN; In N,N-dimethyl-formamide;

DOI:10.1246/bcsj.45.3196

Reference yield: 91.0%

9H-fluorene-9-oxo-2-carbossamide (3096-44-4) → fluorenone-2-carboxylic acid (784-50-9)

Guidance literature:

With sodium hydroxide; In ethanol; water; at 110 ℃; for 6h;

DOI:10.1016/j.bmc.2016.09.041

upstream raw materials:

2-iodo-9H-fluorene

Downstream raw materials:

fluorenone-2-carboxylic acid