ACETALDEHYDE SODIUM BISULFITE

Base Information

• Chemical Name: ACETALDEHYDE SODIUM BISULFITE
• CAS No.: 918-04-7
• Molecular Formula: C2H6 O4 S . Na
• Molecular Weight: 148.115
• Mol file: 918-04-7.mol

Synonyms:Ethanesulfonicacid, 1-hydroxy-, monosodium salt (8CI,9CI); Ethanesulfonic acid, 1-hydroxy-,sodium salt (6CI,7CI); Acetaldehyde sodium bisulfite; Acetaldehyde sodiumbisulfite adduct; Acetaldehyde-sodium bisulfite compound; Sodium1-hydroxyethanesulfonate

Chemical Property of ACETALDEHYDE SODIUM BISULFITE

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 85.81000
• Density: g/cm³
• LogP: -0.04930

Purity/Quality:

99.9% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ACETALDEHYDE SODIUM BISULFITE

There total 4 articles about ACETALDEHYDE SODIUM BISULFITE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

acetaldehyde (75-07-0,9002-91-9) → potassium 1-hydroxyethane-1-sulfonate (918-04-7)

Guidance literature:

With sodium metabisulfite; water; In ethanol; Inert atmosphere;

DOI:10.1021/jo3023878

Reference yield:

C12H21O6S(1-)*Na(1+) → L-menthyl glyoxylate monohydrate (111969-64-3) + potassium 1-hydroxyethane-1-sulfonate (918-04-7)

Guidance literature:

With acetaldehyde; In cyclohexane; at 0 - 40 ℃; for 2.5h;

Reference yield:

Glyoxilic acid (298-12-4) → potassium 1-hydroxyethane-1-sulfonate (918-04-7)

Guidance literature:

With sodium hydrogensulfite; In water; at 20 - 30 ℃;

upstream raw materials:

acetaldehyde

Glyoxilic acid

Downstream raw materials:

3-amino-2-methylimidazo[1,2-a]pyridine

N-ethyl-N-phenylamine

acetaldehyde

sodium 1-anilinoethanesulfonate

Refernces

• 1、 Shriner, R. L.,Land, A. H.. "". . p. 888 - 894. Retrieved 1941.
• 2、 Faul, Margaret,Larsen, Rob,Levinson, Adam,Tedrow, Jason,Vounatsos, Filisaty. "Direct reductive amination of aldehyde bisulfite adducts induced by 2-picoline borane: Application to the synthesis of a DPP-IV inhibitor". . p. 1655 - 1659. Retrieved 2013/03/28.