Technology Process of 2,4-Difluoronitrobenzene
There total 28 articles about 2,4-Difluoronitrobenzene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
trihexyl (tetradecyl) phosphonium tetrafluoroborate; potassium fluoride;
In
dimethyl sulfoxide;
at 180 ℃;
for 1.8h;
DOI:10.1016/j.cattod.2012.02.063
- Guidance literature:
-
With
15-crown-5; sodium fluoride;
In
neat (no solvent);
at 150 - 160 ℃;
Catalytic behavior;
- Guidance literature:
-
With
1,1,1,3',3',3'-hexafluoro-propanol; 2-nitrobenzo[d]isothiazol-3(2H)-one 1,1-dioxide;
at 60 ℃;
for 19h;
Inert atmosphere;
Schlenk technique;
DOI:10.1021/acs.orglett.0c00671