bicyclo[3.2.2]non-6-ene

Base Information

• Chemical Name: bicyclo[3.2.2]non-6-ene
• CAS No.: 7124-86-9
• Molecular Formula: C9H14
• Molecular Weight: 122.2075
• Mol file: 7124-86-9.mol

Synonyms:

Chemical Property of bicyclo[3.2.2]non-6-ene

Chemical Property:

• Vapor Pressure: 2.59mmHg at 25°C
• Boiling Point: 164.4°Cat760mmHg
• Flash Point: 37.8°C
• Density: 0.912g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of bicyclo[3.2.2]non-6-ene

There total 7 articles about bicyclo[3.2.2]non-6-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Bicyclo-<3.2.2>-nonan-2,3-dicarbonsaeure (99861-64-0) → Bicyclo<3.2.2>non-6-en (7124-86-9)

Guidance literature:

With lead(IV) acetate; oxygen; In pyridine;

DOI:10.1016/S0040-4020(01)92945-X

Reference yield:

4-Oxa-tricyclo[5.3.2.02,6]dodecane-3,5-dione → Bicyclo<3.2.2>non-6-en (7124-86-9)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. NaOH / aq. HCl

2: Pb(OAc)4, Py / benzene

With pyridine; lead(IV) acetate; sodium hydroxide; In hydrogenchloride; benzene;

DOI:10.1021/jo00815a027

Reference yield:

(1R,2R,6S,7S)-4-Oxa-tricyclo[5.3.2.02,6]dodecane-3,5-dione → Bicyclo<3.2.2>non-6-en (7124-86-9)

Guidance literature:

Multistep reaction; (i) aq. NaOH, (ii) Pb(OAc)4, Py;

DOI:10.1021/ja00840a048

upstream raw materials:

Bicyclo-<3.2.2>-nonan-2,3-dicarbonsaeure

bicyclo[3.2.2]nonane-dicarboxylic acid-(6exo.7exo)

Cyclohepta-1,3-diene

ethyl acrylate

Downstream raw materials:

Bicyclo<3.2.2>nonan