2-(N-ethylanilino)ethyl 2-methylprop-2-enoate

Base Information

• Chemical Name: 2-(N-ethylanilino)ethyl 2-methylprop-2-enoate
• CAS No.: 2997-87-7
• Molecular Formula: C14H19NO2
• Molecular Weight: 233.31
• Mol file: 2997-87-7.mol

Synonyms:

Chemical Property of 2-(N-ethylanilino)ethyl 2-methylprop-2-enoate

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(N-ethylanilino)ethyl 2-methylprop-2-enoate

There total 5 articles about 2-(N-ethylanilino)ethyl 2-methylprop-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2-( N-ethylanilino)ethanol (92-50-2) + methacrylic acid methyl ester (80-62-6,114512-63-9,143476-91-9,25188-98-1,9011-14-7) → N-ethyl-N-(2-methacryloyloxyethyl)aniline (2997-87-7)

Guidance literature:

With potassium phosphate; 4-methoxy-phenol; at 70 ℃; under 225.023 Torr;

Reference yield: 86.0%

2-( N-ethylanilino)ethanol (92-50-2) + Methacryloyl chloride (920-46-7,26937-45-1) → N-ethyl-N-(2-methacryloyloxyethyl)aniline (2997-87-7)

Guidance literature:

With triethylamine; In dichloromethane; for 3h; Cooling with ice;

DOI:10.1039/c4tc00996g

Reference yield:

2-( N-ethylanilino)ethanol (92-50-2) + dioctyltin(IV) oxide (870-08-6) + methacrylic acid methyl ester (80-62-6,114512-63-9,143476-91-9,25188-98-1,9011-14-7) → N-ethyl-N-(2-methacryloyloxyethyl)aniline (2997-87-7)

Guidance literature:

In dichloromethane; toluene;

upstream raw materials:

2-( N-ethylanilino)ethanol

methacrylic acid methyl ester

dioctyltin(IV) oxide

Methacryloyl chloride

Refernces

• 1、 -. "(Meth) acrylic acid ester manufacturing method of N, N-substituted amino alcohol". Paragraph 0081-0083. . Retrieved 2017/02/23.
• 2、 -. "PROCESS FOR PREPARING (METH)ACRYLIC ESTERS OF N,N-SUBSTITUTED AMINO ALCOHOLS". Page/Page column 5. . Retrieved 2012/04/05.