1-Naphthalenecarboxylic acid, propyl ester

Base Information

• Chemical Name: 1-Naphthalenecarboxylic acid, propyl ester
• CAS No.: 3007-96-3
• Molecular Formula: C14H14O2
• Molecular Weight: 214.264
• Mol file: 3007-96-3.mol

Synonyms:

Chemical Property of 1-Naphthalenecarboxylic acid, propyl ester

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Naphthalenecarboxylic acid, propyl ester

There total 1 articles about 1-Naphthalenecarboxylic acid, propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(2-(naphthalen-1-yl)ethynyl)benzaldehyde (1180487-37-9) → 1,3-diiodo-2-phenylnaphthalene (1370697-43-0) + propyl naphthalene-1-carboxylate (3007-96-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: ethylmagnesium bromide / tetrahydrofuran / 0.5 h / 40 °C

1.2: 23 - 25 °C

2.1: Iodine monochloride / 23 - 25 °C

With ethylmagnesium bromide; Iodine monochloride; In tetrahydrofuran;

DOI:10.1021/ol300457c

Reference yield:

propyl naphthalene-1-carboxylate (3007-96-3) → 1-Cyanonaphthalene (86-53-3)

Guidance literature:

propyl naphthalene-1-carboxylate; With sodium diisobutyl-tert-butoxyaluminium hydride; In tetrahydrofuran; at -40 - 0 ℃; for 4h; Inert atmosphere;

With ammonium hydroxide; iodine; In tetrahydrofuran; at 0 - 20 ℃; for 2h; Inert atmosphere;

DOI:10.1002/ejoc.201300629

upstream raw materials:

2-(2-(naphthalen-1-yl)ethynyl)benzaldehyde

Downstream raw materials:

1-Cyanonaphthalene

Refernces