Borinic acid, diphenylthio-, ethyl ester

Base Information Edit

Chemical Name:Borinic acid, diphenylthio-, ethyl ester
CAS No.:31179-14-3
Molecular Formula:C14H15BS
Molecular Weight:226.15
Hs Code.:
Mol file:31179-14-3.mol

Synonyms:

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Chemical Property of Borinic acid, diphenylthio-, ethyl ester Edit

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of Borinic acid, diphenylthio-, ethyl ester

There total 2 articles about Borinic acid, diphenylthio-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 3677-81-4
diphenylboronchloride

: 28420-40-8,32812-83-2,40597-30-6
lead(II) ethyl sulfide

: 31179-14-3
(C₆H₅)2BSC₂H₅

Guidance literature:: DOI:10.1016/0022-1902(73)80057-0

Reference yield: 80.0%

: 5123-17-1
bromodiphenylborane

: 75-08-1
ethanethiol

: 31179-14-3
(C₆H₅)2BSC₂H₅

Guidance literature:: With triethylamine; In carbon disulfide; flask is charged with CS2 and ethanethiol and cooled in ice-bath, borane is added dropwise with stirring, Et3N is added subsequently, mixt. is slowly warmed to room temp., then refluxed for 4 h; cooling to room temp., filtn., evapn., rectification, elem. anal.;