N,N-Dimethylformamide dicyclohexyl acetal

Base Information

• Chemical Name: N,N-Dimethylformamide dicyclohexyl acetal
• CAS No.: 2016-05-9
• Molecular Formula: C15H29NO2
• Molecular Weight: 255.401
• Hs Code.: 2922199090
• European Community (EC) Number: 217-947-2
• DSSTox Substance ID: DTXSID90942208
• Nikkaji Number: J199.823D
• Wikidata: Q82919175
• Mol file: 2016-05-9.mol

Synonyms:N,N-Dimethylformamide dicyclohexyl acetal;2016-05-9;1,1-dicyclohexyloxy-N,N-dimethylmethanamine;[bis(cyclohexyloxy)methyl]dimethylamine;1,1-bis(cyclohexyloxy)-N,N-dimethylmethanamine;Methanamine, 1,1-bis(cyclohexyloxy)-N,N-dimethyl-;SCHEMBL134671;DTXSID90942208;CHEBI:189236;EINECS 217-947-2;1,1-Bis(cyclohexyloxy)trimethylamine;AKOS015916037;N-[Bis(cyclohexyloxy)methyl]-N,N-dimethylamine #;J-013072

Chemical Property of N,N-Dimethylformamide dicyclohexyl acetal

Chemical Property:

• Vapor Pressure: 0.000596mmHg at 25°C
• Refractive Index: n20/D 1.4678(lit.)
• Boiling Point: 310.5 °C at 760 mmHg
• Flash Point: 90.6 °C
• PSA: 21.70000
• Density: 0.98 g/cm³
• LogP: 3.53020
• XLogP3: 3.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 5
• Exact Mass: 255.219829168
• Heavy Atom Count: 18
• Complexity: 201

Purity/Quality:

99% ^*data from raw suppliers

N,N-Dimethylformamidedicyclohexylacetal 99% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)C(OC1CCCCC1)OC2CCCCC2

Technology Process of N,N-Dimethylformamide dicyclohexyl acetal

There total 4 articles about N,N-Dimethylformamide dicyclohexyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N-dimethyl-formamide (68-12-2,33513-42-7) + cyclohexanol (108-93-0) → dimethylformamide di-cyclohexyl acetal (2016-05-9)

Guidance literature:

Multistep reaction; (i) SOCl₂, (ii) /BRN= 906744/, Na, CHCl₃;

DOI:10.1002/jps.2600600116

Reference yield:

N,N-dimethyl-formamide dimethyl acetal (4637-24-5) + cyclohexanol (108-93-0) → dimethylformamide di-cyclohexyl acetal (2016-05-9)

Guidance literature:

Reference yield:

(bis-ethylsulfanyl-methyl)-dimethyl-amine (5780-17-6) + cyclohexanol (108-93-0) → dimethylformamide di-cyclohexyl acetal (2016-05-9)

Guidance literature:

DOI:10.1007/BF00846003

upstream raw materials:

N,N-dimethyl-formamide dimethyl acetal

cyclohexanol

N,N-dimethyl-formamide

(bis-ethylsulfanyl-methyl)-dimethyl-amine

Downstream raw materials:

3,4,6-Tri-O-acetyl-1,2-O-<1-(exo-cyclohexyloxy)ethylidene>-α-D-glucopyranose

(E)-3-(dimethylamino)-1-(3-(trifluoromethyl)phenyl)prop-2-en-1-one

3-(4-cyanobenzoyl) indolizine

(Bis-cyclohexyloxy-methyl)-phosphonic acid diethyl ester

Refernces