Methyl 3-((3-oxobutyl)sulfonyl)propanoate

Base Information

• Chemical Name: Methyl 3-((3-oxobutyl)sulfonyl)propanoate
• CAS No.: 502635-00-9
• Molecular Formula: C8H14O5S
• Molecular Weight: 222.25900
• Hs Code.: 2918300090
• Mol file: 502635-00-9.mol

Synonyms:Methyl 3-((3-oxobutyl)sulfonyl)propanoate;

Chemical Property of Methyl 3-((3-oxobutyl)sulfonyl)propanoate

Chemical Property:

• PSA: 85.89000
• LogP: 1.02420

Purity/Quality:

98%,99%, ^*data from raw suppliers

Methyl 3-((3-oxobutyl)sulfonyl)propanoate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methyl 3-((3-oxobutyl)sulfonyl)propanoate

There total 1 articles about Methyl 3-((3-oxobutyl)sulfonyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

methyl 3-[(3-oxobutyl)thio]propanoate → methyl 3-[(3-oxobutyl)sulfonyl]propanoate (502635-00-9)

Guidance literature:

With sodium tungstate; dihydrogen peroxide; Aliquat 336; In cyclohexane; water; ethyl acetate; at 60 ℃; for 4h;

DOI:10.1016/S0040-4039(02)02073-7

Reference yield: 92.0%

methyl 3-[(3-oxobutyl)sulfonyl]propanoate (502635-00-9) → sodium 3-methoxy-3-oxo-propane-1-sulfinate (90030-48-1)

Guidance literature:

With sodium methylate; In tetrahydrofuran; methanol; at 20 ℃; for 0.25h;

DOI:10.1016/S0040-4039(02)02073-7

Downstream raw materials:

sodium 3-methoxy-3-oxo-propane-1-sulfinate

Refernces

• 1、 Baskin, Jeremy M,Wang, Zhaoyin. "A mild, convenient synthesis of sulfinic acid salts and sulfonamides from alkyl and aryl halides". . p. 8479 - 8483. Retrieved 2007/10/03.