1-BroMo-3-broMoMethyl-5-Methyl-benzene

Base Information

• Chemical Name: 1-BroMo-3-broMoMethyl-5-Methyl-benzene
• CAS No.: 51719-69-8
• Molecular Formula: C8H8Br2
• Molecular Weight: 263.96
• Hs Code.: 2909309090
• Mol file: 51719-69-8.mol

Synonyms:1-bromo-3-bromomethyl-5-methylbenzene;1-bromo-3-bromomethyl-5-methyl-benzene;3-bromo-5-methylbenzyl bromide;1-BROMO-3-(BROMOMETHYL)-5-METHYLBENZENE;

Chemical Property of 1-BroMo-3-broMoMethyl-5-Methyl-benzene

Chemical Property:

• PSA: 0.00000
• LogP: 3.65240

Purity/Quality:

3-Bromo-5-methylbenzyl bromide 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-BroMo-3-broMoMethyl-5-Methyl-benzene

There total 5 articles about 1-BroMo-3-broMoMethyl-5-Methyl-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

5-bromo-1,3-xylene (556-96-7) → 1-bromo-3-(bromomethyl)-5-methylbenzene (51719-69-8)

Guidance literature:

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; for 2h; Heating / reflux;

Reference yield: 80.1%

→ 1-bromo-3-(bromomethyl)-5-methylbenzene (51719-69-8)

Guidance literature:

With N-Bromosuccinimide; dibenzoyl peroxide; In dichloromethane; for 12h; Reflux;

Reference yield: 49.0%

5-bromo-1,3-xylene (556-96-7) → 1-bromo-3-bromomethyl-5-dibromomethyl-benzene + 1-bromo-3,5-bis(bromomethyl)benzene (51760-23-7) + 1-bromo-3-(bromomethyl)-5-methylbenzene (51719-69-8)

Guidance literature:

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In dichloromethane; for 30.5h; Reflux;

DOI:10.5802/crchim.99

upstream raw materials:

5-bromo-1,3-xylene

dibenzoyl peroxide

Downstream raw materials:

2-(3-bromo-5-methylphenyl)acetonitrile

3-bromo-5-methylbenzaldehyde

1-bromo-3,5-bis(diethoxyphosphorylmethyl)benzene

C₁₈H₁₈N₄

Refernces

• 1、 -. "Novel phenanthrene compounds, a method of making the same and organic electronic devices using the same". Paragraph 0236-0239; 0476-0479. . Retrieved 2019/10/22.
• 2、 -. "ANILINE DERIVATIVES,THEIR PREPARATION AND THEIR THERAPEUTIC APPLICATION". Page/Page column 55. . Retrieved 2013/03/28.